Upgradation of bauxite by molecular hydrogen and hydrogen plasma

B. R. Parhi, S. K. Sahoo, S. C. Mishra, B. Bhoi, R. K. Paramguru, B. K. Satapathy

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    Cite this article as:

    B. R. Parhi, S. K. Sahoo, S. C. Mishra, B. Bhoi, R. K. Paramguru, and B. K. Satapathy, Upgradation of bauxite by molecular hydrogen and hydrogen plasma, Int. J. Miner. Metall. Mater., 23(2016), No. 10, pp.1141-1149. https://dx.doi.org/10.1007/s12613-016-1333-x
    B. R. Parhi, S. K. Sahoo, S. C. Mishra, B. Bhoi, R. K. Paramguru, and B. K. Satapathy, Upgradation of bauxite by molecular hydrogen and hydrogen plasma, Int. J. Miner. Metall. Mater., 23(2016), No. 10, pp.1141-1149. https://dx.doi.org/10.1007/s12613-016-1333-x
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    Upgradation of bauxite by molecular hydrogen and hydrogen plasma

    基金项目: 

    The authors would like to thank the National Aluminium Company (NALCO) for financial support. They also would like to thank Mr. M. Agarwal of SLM Metal (P) Ltd., Rourkela, and Prof. B.K. Mishra, director of Institute of Minerals and Materials Technology (IMMT), Bhubaneswar, for allowing us to conduct the reduction processing of bauxite samples. One author of this manuscript, Mr. B.R. Parhi, would like to thank Dr. R. Bhima Rao, former scientist, and Dr. B.C. Tripathy, scientist, IMMT, Bhubaneswar, for their valuable suggestions while preparing the manuscript.

      通信作者:

      B. R. Parhi E-mail: basudevpurbikash@gmail.com

    An approach was developed to upgrade the bauxite ore by molecular hydrogen and hydrogen plasma. A gibbsite-type bauxite sample was obtained from National Aluminium Company (NALCO), Odisha, India. The obtained sample was crushed and sieved (to 100 μm) prior to the chemical analysis and grain-size distribution study. The bauxite sample was calcined in the temperature range from 500 to 700°C for different time intervals to optimize the conditions for maximum moisture removal. This process was followed by the reduction of the calcined ore by molecular hydrogen and hydrogen plasma. Extraction of alumina from the reduced ore was carried out via acid leaching in chloride media for 2 h at 60°C. X-ray diffraction, scanning electron microscopy, thermogravimetry in conjunction with differential scanning calorimetry, and Fourier transform infrared spectroscopy were used to determine the physicochemical characteristics of the material before and after extraction. Alumina extracted from the reduced ore at the optimum calcination temperature of 700°C and the optimum calcination time of 4 h is found to be 90% pure.

     

    Upgradation of bauxite by molecular hydrogen and hydrogen plasma

    Author Affilications
    • Funds: 

      The authors would like to thank the National Aluminium Company (NALCO) for financial support. They also would like to thank Mr. M. Agarwal of SLM Metal (P) Ltd., Rourkela, and Prof. B.K. Mishra, director of Institute of Minerals and Materials Technology (IMMT), Bhubaneswar, for allowing us to conduct the reduction processing of bauxite samples. One author of this manuscript, Mr. B.R. Parhi, would like to thank Dr. R. Bhima Rao, former scientist, and Dr. B.C. Tripathy, scientist, IMMT, Bhubaneswar, for their valuable suggestions while preparing the manuscript.

    • Received: 06 January 2016; Revised: 08 April 2016; Accepted: 21 May 2016;
    An approach was developed to upgrade the bauxite ore by molecular hydrogen and hydrogen plasma. A gibbsite-type bauxite sample was obtained from National Aluminium Company (NALCO), Odisha, India. The obtained sample was crushed and sieved (to 100 μm) prior to the chemical analysis and grain-size distribution study. The bauxite sample was calcined in the temperature range from 500 to 700°C for different time intervals to optimize the conditions for maximum moisture removal. This process was followed by the reduction of the calcined ore by molecular hydrogen and hydrogen plasma. Extraction of alumina from the reduced ore was carried out via acid leaching in chloride media for 2 h at 60°C. X-ray diffraction, scanning electron microscopy, thermogravimetry in conjunction with differential scanning calorimetry, and Fourier transform infrared spectroscopy were used to determine the physicochemical characteristics of the material before and after extraction. Alumina extracted from the reduced ore at the optimum calcination temperature of 700°C and the optimum calcination time of 4 h is found to be 90% pure.

     

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