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Volume 24 Issue 5
May  2017
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Hui-bin Wu, Gang Niu, Feng-juan Wu, and Di Tang, Reverse-transformation austenite structure control with micro/nanometer size, Int. J. Miner. Metall. Mater., 24(2017), No. 5, pp. 530-537. https://doi.org/10.1007/s12613-017-1434-1
Cite this article as:
Hui-bin Wu, Gang Niu, Feng-juan Wu, and Di Tang, Reverse-transformation austenite structure control with micro/nanometer size, Int. J. Miner. Metall. Mater., 24(2017), No. 5, pp. 530-537. https://doi.org/10.1007/s12613-017-1434-1
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研究论文Open Access

Reverse-transformation austenite structure control with micro/nanometer size

  • 通讯作者:

    Gang Niu    E-mail: ustbning@163.com

  • To control the reverse-transformation austenite structure through manipulation of the micro/nanometer grain structure, the influences of cold deformation and annealing parameters on the microstructure evolution and mechanical properties of 316L austenitic stainless steel were investigated. The samples were first cold-rolled, and then samples deformed to different extents were annealed at different temperatures. The microstructure evolutions were analyzed by optical microscopy, scanning electron microscopy (SEM), magnetic measurements, and X-ray diffraction (XRD); the mechanical properties are also determined by tensile tests. The results showed that the fraction of stain-induced martensite was approximately 72% in the 90% cold-rolled steel. The micro/nanometric microstructure was obtained after reversion annealing at 820-870℃ for 60 s. Nearly 100% reversed austenite was obtained in samples annealed at 850℃, where grains with a diameter ≤ 500 nm accounted for 30% and those with a diameter >0.5 μm accounted for 70%. The micro/nanometer-grain steel exhibited not only a high strength level (approximately 959 MPa) but also a desirable elongation of approximately 45%.
  • Research ArticleOpen Access

    Reverse-transformation austenite structure control with micro/nanometer size

    + Author Affiliations
    • To control the reverse-transformation austenite structure through manipulation of the micro/nanometer grain structure, the influences of cold deformation and annealing parameters on the microstructure evolution and mechanical properties of 316L austenitic stainless steel were investigated. The samples were first cold-rolled, and then samples deformed to different extents were annealed at different temperatures. The microstructure evolutions were analyzed by optical microscopy, scanning electron microscopy (SEM), magnetic measurements, and X-ray diffraction (XRD); the mechanical properties are also determined by tensile tests. The results showed that the fraction of stain-induced martensite was approximately 72% in the 90% cold-rolled steel. The micro/nanometric microstructure was obtained after reversion annealing at 820-870℃ for 60 s. Nearly 100% reversed austenite was obtained in samples annealed at 850℃, where grains with a diameter ≤ 500 nm accounted for 30% and those with a diameter >0.5 μm accounted for 70%. The micro/nanometer-grain steel exhibited not only a high strength level (approximately 959 MPa) but also a desirable elongation of approximately 45%.
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    • [1]
      R.D.K. Misra, W.W. Thein-Han, T.C. Pesacreta, M.C. Somani, and L.P. Karjalainen, Biological significance of nanograined/ultrafine-grained structures:Interaction with fibroblasts, Acta Biomater., 6(2010), No. 8, p. 3339.
      [2]
      R.D.K. Misra, W.W. Thein-Han, S.A. Mali, M.C. Somani, and L.P. Karjalainen, Cellular activity of bioactive nanograined/ultrafine-grained materials, Acta Biomater., 6(2010), No. 7, p. 2826.
      [3]
      S. Mali, R.D.K. Misra, M.C. Somani, and L.P. Karjalainen, Biomimetic nanostructured coatings on nano-grained/ultrafine-grained substrate:microstructure, surface adhesion strength, and biosolubility, Mater. Sci. Eng. C, 29(2009), No. 8, p. 2417.
      [4]
      P.K.C. Venkatsurya, W.W. Thein-Han, R.D.K. Misra, M.C. Somani, and L.P. Karjalainen, Advancing nanograined/ultrafine-grained structures for metal implant technology:interplay between grooving of nano/ultrafine grains and cellular response, Mater. Sci. Eng. C, 30(2010), No. 7, p. 1050.
      [5]
      R.D.K. Misra, B.R. Kumar, M. Somani, and P. Karjalainen, Deformation processes during tensile straining of ultrafine/nanograined structures formed by reversion in metastable austenitic steels, Scripta Mater., 59(2008), No. 1, p. 79.
      [6]
      B. Hwang and C.G. Lee, Influence of thermomechanical processing and heat treatments on tensile and Charpy impact properties of B and Cu bearing high-strength low-alloy steels, Mater. Sci. Eng. A, 527(2010), No. 16-17, p. 4341.
      [7]
      X.W. Kong, L.Y. Lan, Z.Y. Hu, B. Li, and T.Z. Sui, Optimization of mechanical properties of high strength bainitic steel using thermo-mechanical control and accelerated cooling process, J. Mater. Process. Technol., 217(2015), p. 202.
      [8]
      H.X. Yin, A.M. Zhao, Z.Z. Zhao, X. Li, S.J. Li, H.J. Hu, and W.G. Xia, Influence of original microstructure on the transformation behavior and mechanical properties of ultra-high-strength TRIP-aided steel, Int. J. Miner. Metall. Mater., 22(2015), No. 3, p. 262.
      [9]
      T. Sakai, A. Belyakov, R. Kaibyshev, H. Miura, and J.J. Jonas, Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions, Prog. Mater Sci., 60(2014), p. 130.
      [10]
      I.A. Yakubtsov, P. Poruks, and J.D. Boyd, Microstructure and mechanical properties of bainitic low carbon high strength plate steels, Mater. Sci. Eng. A, 480(2008), No. 1-2, p. 109.
      [11]
      X.X. Xu, Y. Yu, W.L. Cui, B.Z. Bai, and J.L. Gu, Ultra-high cycle fatigue behavior of high strength steel with carbide-free bainite/martensite complex microstructure, Int. J. Miner. Metall. Mater., 16(2009), No. 3, p. 285.
      [12]
      Y.Q. Weng, achievements of new generation steels program in china, Mater. Rev., 18(2004), p. 68.
      [13]
      M.M. Tong, J. Ni, Y.T. Zhang, D.Z. Li, and Y.Y. Li, Temporal oscillatory behavior in deformation induced ferrite transformation in an Fe-C binary system, Scripta Mater., 50(2004), No. 6, p. 909.
      [14]
      C. Garcia-Mateo, F.G. Caballero, and H.K.D.H. Bhadeshia, Development of hard bainite, ISIJ Int., 43(2003), No. 8, p. 1238.
      [15]
      F. Forouzan, A. Najafizadeh, A. Kermanpur, A. Hedayati, and R. Surkialiabad, Production of nano/submicron grained AISI 304L stainless steel through the martensite reversion process, Mater. Sci. Eng. A, 527(2010), No. 27, p. 7334.
      [16]
      R. Ueji, N. Tsuji, Y. Minamino, and Y. Koizumi, Ultragrain refinement of plain low carbon steel by cold-rolling and annealing of martensite, Acta Mater., 50(2002), No. 16, p. 4177.
      [17]
      W. Jiang, D. Ye, J. Li, J. Su, and K.Y. Zhao, Reverse transformation mechanism of martensite to austenite in 00Cr15Ni7Mo2WCu2 super martensitic stainless steel, Steel Res. Int., 85(2014), No. 7, p. 1150.
      [18]
      C. Ghosh, C. Aranas Jr., and J.J. Jonas, Dynamic transformation of deformed austenite at temperatures above the Ae3, Prog. Mater Sci., 82(2016), p. 151.
      [19]
      K. Tomimura, S. Takaki, and Y. Tokunaga, Reversion mechanism from deformation induced martensite to austenite in metastable austenitic stainless steels, ISIJ Int., 31(1991), No. 12, p. 1431.
      [20]
      A. Belyakov, K. Tsuzaki, H. Miura, and T. Sakai, Effect of initial microstructures on grain refinement in a stainless steel by large strain deformation, Acta Mater., 51(2003), No. 3, p. 847.
      [21]
      J. Han and Y.K. Lee, The effects of the heating rate on the reverse transformation mechanism and the phase stability of reverted austenite in medium Mn steels, Acta Mater., 67(2014), p. 354.

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