Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel

Jin-tao Shi; Long-gang Hou; Jin-rong Zuo; Lin-zhong Zhuang; Ji-shan Zhang

doi:10.1007/s12613-017-1446-x

Volume 24 Issue 6

Jun. 2017

Turn off MathJax

数据统计

计量

文章访问数: 416
HTML全文浏览量: 44
PDF下载量: 22
被引次数: 0

文章导航 > 矿物冶金与材料学报（英文） > 2017 > 24(6): 638-645

Jin-tao Shi, Long-gang Hou, Jin-rong Zuo, Lin-zhong Zhuang, and Ji-shan Zhang, Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel, Int. J. Miner. Metall. Mater., 24(2017), No. 6, pp. 638-645. https://doi.org/10.1007/s12613-017-1446-x

Cite this article as:

Jin-tao Shi, Long-gang Hou, Jin-rong Zuo, Lin-zhong Zhuang, and Ji-shan Zhang, Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel, Int. J. Miner. Metall. Mater., 24(2017), No. 6, pp. 638-645. https://doi.org/10.1007/s12613-017-1446-x

Citation:

PDF( 1487 KB)

引用本文 PDF XML SpringerLink

研究论文

Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel

State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083, China

通讯作者:
Long-gang Hou E-mail: lghou@skl.ustb.edu.cn

Ji-shan Zhang E-mail: zhangjs@skl.ustb.edu.cn

中文摘要

Metastable 304 austenitic stainless steel was subjected to rolling at cryogenic and room temperatures, followed by annealing at different temperatures from 500 to 950℃. Phase transition during annealing was studied using X-ray diffractometry. Transmission electron microscopy and electron backscattered diffraction were used to characterize the martensite transformation and the distribution of austenite grain size after annealing. The recrystallization mechanism during cryogenic rolling was a reversal of martensite into austenite and austenite growth. Cryogenic rolling followed by annealing refined grains to 4.7 μm compared with 8.7 μm achieved under room-temperature rolling, as shown by the electron backscattered diffraction images. Tensile tests showed significantly improved mechanical properties after cryogenic rolling as the yield strength was enhanced by 47% compared with room-temperature rolling.

关键词:

Research Article

Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel

+ Author Affiliations

Abstract

Abstract

Metastable 304 austenitic stainless steel was subjected to rolling at cryogenic and room temperatures, followed by annealing at different temperatures from 500 to 950℃. Phase transition during annealing was studied using X-ray diffractometry. Transmission electron microscopy and electron backscattered diffraction were used to characterize the martensite transformation and the distribution of austenite grain size after annealing. The recrystallization mechanism during cryogenic rolling was a reversal of martensite into austenite and austenite growth. Cryogenic rolling followed by annealing refined grains to 4.7 μm compared with 8.7 μm achieved under room-temperature rolling, as shown by the electron backscattered diffraction images. Tensile tests showed significantly improved mechanical properties after cryogenic rolling as the yield strength was enhanced by 47% compared with room-temperature rolling.
- stainless steel;
- cryogenic rolling;
- annealing;
- microstructural evolution;
- mechanical properties;
- recrystallization

FullText(HTML)

Supplements(0)

References(37)

References

[1]	C. Herrera, R.L. Plaut, and A.F. Padilha, Microstructural refinement during annealing of plastically deformed austenitic stainless steels, Mater. Sci. Forum, 550(2007), p. 423.
[2]	B.R. Kumar, S.K. Das, B. Mahato, and R.N. Ghosh, Role of strain-induced martensite on microstructural evolution during annealing of metastable austenitic stainless steel, J. Mater. Sci., 45(2010), No. 4, p. 911.
[3]	A.F. Padilha, R.L. Plaut, and P.R. Rios, Annealing of cold-worked austenitic stainless steels, ISIJ Int., 43(2003), No. 2, p. 135.
[4]	R.D.K. Misra, Z. Zhang, P.K.C. Venkatasurya, M.C. Somani, and L.P. Karjalainen, The effect of nitrogen on the formation of phase reversion-induced nanograined/ultrafine-grained structure and mechanical behavior of a Cr-Ni-N steel, Mater. Sci. Eng. A, 528(2011), No. 3, p. 1889.
[5]	R.Z. Valiev, N.A. Krasilnikov, and N.K. Tsenev, Plastic deformation of alloys with submicron-grained structure, Mater. Sci. Eng. A, 137(1991), p. 35.
[6]	D. Jia, Y.M. Wang, K.T. Ramesh, E. Ma, Y.T. Zhu, and R.Z. Valiev, Deformation behavior and plastic instabilities of ultrafine-grained titanium, Appl. Phys. Lett., 79(2001), No. 5, p. 611.
[7]	Y. Iwahashi, J.T. Wang, Z. Horita, M. Nemoto, and T.G. Langdon, Principle of equal-channel angular pressing for the processing of ultra-fine grained materials, Scripta Mater., 35(1996), No. 2, p. 143.
[8]	Y. Ivanisenko, R.K. Wunderlich, R.Z. Valiev, and H.J. Fecht, Annealing behaviour of nanostructured carbon steel produced by severe plastic deformation, Scripta Mater., 49(2003), No. 10, p. 947.
[9]	F.K. Yan, N.R. Tao, and K. Lu, Tensile ductility of nanotwinned austenitic grains in an austenitic steel, Scripta Mater., 84-85(2014), p. 31.
[10]	Y.F. Shen, X.X. Li, X. Sun, Y.D. Wang, and L. Zuo, Twinning and martensite in a 304 austenitic stainless steel, Mater. Sci. Eng. A, 552(2012), p. 514.
[11]	J.L. Lv and H.Y. Luo, Effect of nano/ultrafine grain with orientation obtained by reversion transformation on tensile behaviour of austenitic stainless steel, Mater. Sci. Technol., 29(2013), No. 4, p. 456.
[12]	K.L. Ye, H.Y. Luo, and J.L. Lv, Producing nanostructured 304 stainless steel by rolling at cryogenic temperature, Mater. Manuf. Processes, 29(2014), No. 6, p. 754.
[13]	M.A. Meyers, Y.B. Xu, Q. Xue, M.T. Pérez-Prado, and T.R. McNelley, Microstructural evolution in adiabatic shear localization in stainless steel, Acta Mater., 51(2003), No. 5, p. 1307.
[14]	L. Lu, X.H. Chen, X.X. Huang, and K. Lu, Revealing the maximum strength in nanotwinned copper, Science, 323(2009), No. 5914, p. 607.
[15]	W.S. Lee and C.F. Lin, Comparative study of the impact response and microstructure of 304L stainless steel with and without prestrain, Metall. Trans. A, 33(2002), No. 9, p. 2801.
[16]	W.S. Lee, C.F. Lin, T.H. Chen, and M.C. Yang, High temperature microstructural evolution of 304L stainless steel as function of pre-strain and strain rate, Mater. Sci. Eng. A, 527(2010), No. 13-14, p. 3127.
[17]	P.L. Sun, Y.H. Zhao, J.C. Cooley, M.E. Kassner, Z. Horita, T.G. Langdon, E.J. Lavernia, and Y.T. Zhu, Effect of stacking fault energy on strength and ductility of nanostructured alloys:an evaluation with minimum solution hardening, Mater. Sci. Eng. A, 525(2009), No. 1-2, p. 83.
[18]	B.R. Kumar and D. Raabe, Tensile deformation characteristics of bulk ultrafine-grained austenitic stainless steel produced by thermal cycling, Scripta Mater., 66(2012), No. 9, p. 634.
[19]	S. Sabooni, F. Karimzadeh, M.H. Enayati, and A.H.W. Ngan, The role of martensitic transformation on bimodal grain structure in ultrafine grained AISI 304L stainless steel, Mater. Sci. Eng. A, 636(2015), p. 221.
[20]	J. Das, Evolution of nanostructure in α-brass upon cryorolling, Mater. Sci. Eng. A, 530(2011), No. 1, p. 675.
[21]	B. Roy, N.K. Kumar, P.M.G. Nambissan, and J. Das, Evolution and interaction of twins, dislocations and stacking faults in rolled α-brass during nanostructuring at sub-zero temperature, AIP Adv., 4(2014), No. 6, art. No. 067101.
[22]	N.K. Kumar, B. Roy, and J. Das, Effect of twin spacing, dislocation density and crystallite size on the strength of nanostructured α-brass, J. Alloys Compd., 618(2015), p. 139.
[23]	V.A. Moskalenko, A.R. Smirnov, and R.V. Smolyanets, Low-temperature plastic deformation and strain-hardening of nanocrystalline titanium, Low Temp. Phys., 40(2014), p. 837.
[24]	B. Roy, R. Kumar, and J. Das, Effect of cryorolling on the microstructure and tensile properties of bulk nano-austenitic stainless steel, Mater. Sci. Eng. A, 631(2015), p. 241.
[25]	P.Y. Li, Y. Xiong, L.F. Chen, F.Z. Ren, and X.G. Wang, Effect of cryorolling on microstructure and mechanical properties of AISI 310S stainless steel, Trans. Mater. Heat Treat., 36(2015), No. 3, p. 112.
[26]	Y. Xiong, J.B. Wang, L.F. Chen, Y. Lu, F.Z. Ren, L.L. Zhang, and J.L. Ma, Effect of annealing process on microstructure and mechanical properties of cryorolled AISI310S austenite stainless steel, Trans. Mater. Heat Treat., 37(2016), No. 4, p. 101.
[27]	J.T. Shi, L.G. Hou, J.R. Zuo, L. Lu, H. Cui, and J.S. Zhang, Quantitative analysis of the martensite transformation and microstructure characterization during cryogenic rolling of a 304 austenitic stainless steel, Acta Metall. Sin., 52(2016), No. 8, p. 945.
[28]	N.H. Moser, T.S. Gross, and Y.P. Korkolis, Martensite formation in conventional and isothermal tension of 304 austenitic stainless steel measured by X-ray diffraction, Metall. Mater. Trans. A, 45(2014), No. 11, p. 4891.
[29]	B.D. Cullity and S.R. Stock, Elements of X-ray Diffraction, 3rd Ed., Prentice Hall, New Jersey, 2001, p. 40.
[30]	A.K. De, D.C. Murdock, M.C. Mataya, J.G. Speer, and D.K. Matlock, Quantitative measurement of deformation-induced martensite in 304 stainless steel by X-ray diffraction, Scripta Mater., 50(2004), No. 12, p. 1445.
[31]	X.M. Huang and T. Jie, Material Analysis Test Method, National Defense Industry Press, Beijing, 2008, p. 206.
[32]	Z.Y. Xu, Martensite Transformation and Martensite, Science Press, Beijing, 1980, p. 479.
[33]	T. Shintani and Y. Murata, Evaluation of the dislocation density and dislocation character in cold rolled type 304 steel determined by profile analysis of X-ray diffraction, Acta Mater., 59(2011), No. 11, p. 4314.
[34]	W.M. Mao and X.B. Zhao, Recrystallization and Grain Growth, Metallurgical Industry Press, Beijing, 1994, p. 218.
[35]	F. Forouzan, A. Kermanpur, A. Najafizadeh, and A. Hedayati, Processing of nano/submicron grained stainless steel 304L by an advanced thermomechanical process, Int. J. Mod. Phys. Conf. Ser., 5(2012), p. 383.
[36]	I. Shakhova, V. Dudko, A. Belyakov, K. Tsuzaki, and R. Kaibyshev, Effect of large strain cold rolling and subsequent annealing on microstructure and mechanical properties of an austenitic stainless steel, Mater. Sci. Eng. A, 545(2012), p. 176.
[37]	Y.Q. Ma, J.E. Jin, and Y.K. Lee, A repetitive thermomechanical process to produce nano-crystalline in a metastable austenitic steel, Scripta Mater., 52(2005), No. 12, p. 1311.

Relative Articles

Cited By

Proportional views

数据统计

姓名
邮箱
手机号码
标题
留言内容
验证码

留言板

数据统计

分享

计量

Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel

中文摘要

Effect of cryogenic rolling and annealing on the microstructure evolution and mechanical properties of 304 stainless steel

Abstract

References

数据统计

Catalog