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Volume 24 Issue 10
Oct.  2017
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文章导航 >  矿物冶金与材料学报（英文）  > 2017  >  24(10): 1075-1086
Min Lin, Zhen-yu Pei, Yuan-yuan Liu, Zhang-jie Xia, Kang Xiong, Shao-min Lei, and En-wen Wang, High-efficiency trace Na extraction from crystal quartz ore used for fused silica-A pretreatment technology, Int. J. Miner. Metall. Mater., 24(2017), No. 10, pp. 1075-1086. https://doi.org/10.1007/s12613-017-1498-y
Cite this article as:
Min Lin, Zhen-yu Pei, Yuan-yuan Liu, Zhang-jie Xia, Kang Xiong, Shao-min Lei, and En-wen Wang, High-efficiency trace Na extraction from crystal quartz ore used for fused silica-A pretreatment technology, Int. J. Miner. Metall. Mater., 24(2017), No. 10, pp. 1075-1086. https://doi.org/10.1007/s12613-017-1498-y
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研究论文

High-efficiency trace Na extraction from crystal quartz ore used for fused silica-A pretreatment technology

  • School of Resources and Environmental Engineering, Wuhan University of Technology, Wuhan 430070, China

  • School of Resources and Environmental Engineering, Anshun University, Anshun 561000, China

  • 通讯作者:

    Shao-min Lei    E-mail: shmlei@163.com

  • Trace Na sources, extraction dynamics of trace Na, and influences of calcination temperature on quartz lattice, fluid inclusions, and muscovite were studied in detail herein for trace Na extraction from the quartz ore with water leaching at 90℃. Experimental results suggested that the trace Na sources included quartz lattice, fluid inclusions, and muscovite. The extraction rate of the trace Na in quartz ores can reach 31.0wt% after calcination at 900℃ for 5 h and water leaching at 90℃ for 24 h. The extraction process consisting of the dissolution of unfree Na and diffusion of free Na was dominated by calcination temperature. Calcination at 900℃ for 5 h was effective for extraction of the trace Na in fluid inclusions and muscovite. The extraction of the trace Na was mainly affected by the decrepitation of fluid inclusions when the calcination temperature ranged from 400 to 600℃ and by the damage of muscovite when the calcination temperature ranged from 600 to 900℃. Based on the extraction rates at different calcination temperatures, approximately 20.1wt% of the trace Na occurred in fluid inclusions, approximately 10.9wt% existed in muscovite, and 69.0wt% mainly occurred in quartz lattice.
    • Research Article

    High-efficiency trace Na extraction from crystal quartz ore used for fused silica-A pretreatment technology

    + Author Affiliations
      Abstract
    • Trace Na sources, extraction dynamics of trace Na, and influences of calcination temperature on quartz lattice, fluid inclusions, and muscovite were studied in detail herein for trace Na extraction from the quartz ore with water leaching at 90℃. Experimental results suggested that the trace Na sources included quartz lattice, fluid inclusions, and muscovite. The extraction rate of the trace Na in quartz ores can reach 31.0wt% after calcination at 900℃ for 5 h and water leaching at 90℃ for 24 h. The extraction process consisting of the dissolution of unfree Na and diffusion of free Na was dominated by calcination temperature. Calcination at 900℃ for 5 h was effective for extraction of the trace Na in fluid inclusions and muscovite. The extraction of the trace Na was mainly affected by the decrepitation of fluid inclusions when the calcination temperature ranged from 400 to 600℃ and by the damage of muscovite when the calcination temperature ranged from 600 to 900℃. Based on the extraction rates at different calcination temperatures, approximately 20.1wt% of the trace Na occurred in fluid inclusions, approximately 10.9wt% existed in muscovite, and 69.0wt% mainly occurred in quartz lattice.
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    • [1]
      M.F.M. Santos, E. Fujiwara, E.A. Schenkel, J. Enzweiler, and C.K. Suzuki, Processing of quartz lumps rejected by silicon industry to obtain a raw material for silica glass, Int. J. Miner. Process., 135(2015), p. 65.
      [2]
      N.B. Piperov, L.P. Ivanova, and A.N. Aleksandrova, A reappraisal of decrepitation-inductively coupled plasma spectroscopy (D-ICP) for the bulk analysis of fluid inclusions in minerals, Anal. Methods, 8(2016), No. 15, p. 3183.
      [3]
      H.S. Scott, The decrepitation method applied to minerals with fluid inclusions, Econ. Geol., 43(1948), No. 8, p. 637.
      [4]
      F.G. Smith, Decrepitation characteristics of igneous rocks, Can. Mineral., 6(1957), No. 1, p. 78.
      [5]
      L.Q. Yang, J. Deng, J. Zhang, C.Y. Guo, B.F. Gao, Q.J. Gong, Q.F. Wang, S.Q. Jiang, and H.J. Yu, Decrepitation thermometry and compositions of fluid inclusions of the Damoqujia gold deposit, Jiaodong gold province, China:implications for metallogeny and exploration, J. China Univ. Geosci., 19(2008), No. 4, p. 378.
      [6]
      J.J. Wilkinson, Fluid inclusions in hydrothermal ore deposits, Lithos, 55(2001), No. 1-4, p. 229.
      [7]
      M. Steele-Macinnis, P. Lecumberri-Sanchez, and R.J. Bodnar, Synthetic fluid inclusions XX. Critical PTx properties of H2O-FeCl2 fluids, Geochim. Cosmochim. Acta, 148(2015), p. 50.
      [8]
      K. Burlinson, Acoustic decrepitation as a means of rapidly determining CO2(and other gas) contents in fluid inclusions and its use in exploration, with examples from gold mines in the Shandong and Hubei provinces, China, Acta Petrol. Sinica, 23(2007), No. 1, p. 65.
      [9]
      M.J. Morales, R.C. Figueiredo e Silva, L.M. Lobato, S.D. Gomes, Caio C.C.O. Gomes, and D.A. Banks, Metal source and fluid-rock interaction in the Archean BIF-hosted Lamego gold mineralization:Microthermometric and LA-ICP-MS analyses of fluid inclusions in quartz veins, Rio das Velhas greenstone belt, Brazil, Ore Geol. Rev., 72(2016), p. 510.
      [10]
      S.C. George, H. Volk, and A. Dutkiewicz, Mass Spectrometry Techniques for Analysis of Oil and Gas Trapped in Fluid Inclusions, Handbook of Mass Spectrometry, John Wiley & Sons, Inc., Hoboken, 2012, p. 647.
      [11]
      R. Zhang, H.P. Schwarcz, D.C. Ford, F.S. Schroeder, and P.A. Beddows, An absolute paleotemperature record from 10 to 6 Ka inferred from fluid inclusion D/H ratios of a stalagmite from Vancouver Island, British Columbia, Canada, Geochim. Cosmochim. Acta, 72(2008), No. 4, p. 1014.
      [12]
      M. Campione, N. Malaspina, and M.L. Frezzotti, Threshold size for fluid inclusion decrepitation, J. Geophys. Res. Solid Earth, 120(2015), No. 11, p. 7396.
      [13]
      H.Z. Lu, Y.M. Liu, C.L. Wang, Y.Z. Xu, and H.Q. Li, Mineralization and fluid inclusion study of the shizhuyuan W-Sn-Bi-Mo-F Skarn deposit, Hunan Province, China, Econ. Geol., 98(2003), No. 5, p. 955.
      [14]
      L.J. Wang, H.P. Zhu, and M. Wang, Application of decrepitation method in ore deposits, Geol. Prospect., 43(2007), No. 5, p. 88.
      [15]
      R.J. Bakker and G. Doppler, Salinity and density modifications of synthetic H2O and H2O-NaCl fluid inclusions in re-equilibration experiments at constant temperature and confining pressure, Chem. Geol., 424(2016), p. 73.
      [16]
      I.N. Kigai and B.R. Tagirov, Evolution of acidity of hydrothermal fluids related to hydrolysis of chlorides, Petrology, 18(2010), No. 3, p. 252.
      [17]
      S.A. Ghafri, G.C. Maitland, and J.P.M. Trusle, Densities of aqueous MgCl2(aq), CaCl2(aq), KI (aq), NaCl (aq), KCl (aq), AlCl3(aq), and (0.964 NaCl+0.136 KCl)(aq) at temperatures between (283 and 472) K, pressures up to 68.5 MPa, and molalities up to 6 mol·kg-1, J. Chem. Eng. Data, 57(2012), No. 4, p. 1288.
      [18]
      K. Kemmochi, H. Miyazawa, H. Watanabe, K. Maekawa, C. Tsuji, and M. Saitou, High-Purity Quartz Glass and Method for the Preparation Thereof, American Patent, Appl.5968259 A, 1999.
      [19]
      T. Sato, H. Watanabe, and W. Ponto, Process for Continuous Refining of Quartz Powder, American Patent, Appl.5637284, 1997.
      [20]
      F. Veglió, B. Passariello, M. Barbaro, P. Plescia, and A.M. Marabini, Drum leaching tests in iron removal from quartz using oxalic and sulphuric acids, Int. J. Miner. Process., 54(1998), No. 3-4, p. 183.
      [21]
      I.I. Tarasova, A.W.L. Dudeney, and S. Pilurzu, Glass sand processing by oxalic acid leaching and photocatalytic effluent treatment, Miner. Eng., 14(2001), No. 6, p. 639.
      [22]
      L.T. Rakov, Mechanisms of isomorphic substitution in quartz, Geochem. Int., 44(2006), No. 10, p. 1004.
      [23]
      J.C. Slater, Atomic radii in crystals, J. Chem. Phys., 41(1964), No. 10, p. 3199.
      [24]
      F.L. Yan, Distribution properties and hosting conditions and purification methods of baneful impurity elements in quartz, J. Geol., 33(2009), No. 3, p. 277.
      [25]
      G. Doppler and R.J. Bakker, The influence of the α-β phase transition of quartz on fluid inclusions during re-equilibration experiments, Lithos, 198-199(2014), No. 2, p. 14.
      [26]
      A. Schmidt-Mumm, Low frequency acoustic emission from quartz upon heating from 90 to 610℃, Phys. Chem. Miner., 17(1991), No. 6, p. 545.
      [27]
      M. Thompson, A.H. Rankin, S.J. Walton, C. Halls, and B.N. Foo, The analysis of fluid inclusion decrepitate by inductively-coupled plasma atomic emission spectroscopy:an exploratory study, Chem. Geol., 30(1980), No. 1-2, p. 121.
      [28]
      M. Tschapek, S. Falasca, and C. Wasowski, Quartz sand:Apparent dehydroxylation-rehydroxylation and water retention, J. Plant Nutr. Soil Sci., 147(1984), No. 6, p. 777.
      [29]
      R. Novotny, A. Hoff, and J. Schuertz, Process for Hydrothermal Production of Potassium Silicate Solutions, American Patent, Appl.5084262, 1992.
      [30]
      J.A. Mavrogenes and R.J. Bodnar, Hydrogen movement into and out of fluid inclusions in quartz:experimental evidence and geologic implications, Geochim. Cosmochim. Acta, 58(1994), No. 1, p. 141.
      [31]
      D.L. Hall and S.M. Sterner, Experimental diffusion of hydrogen into synthetic fluid inclusions in quartz, J. Metamorph. Geol., 13(1995), No. 3, p. 345.
      [32]
      K. Krenn, J. Konzett, and G. Hoinkes, Re-equilibration of a high-pressure metamorphic fluid:evidence from tourmaline-, apatite- and quartz-hosted fluid inclusions in an Eoalpine eclogite from the Eastern Alps, Eur. J. Mineral., 26(2014), No. 2, p. 231.
      [33]
      M.O. Vityk and R.J. Bodnar, Do fluid inclusions in high-grade metamorphic terranes preserve peak metamorphic density during retrograde decompression?, Am. Mineral., 80(2015), No. 7-8, p. 641.
      [34]
      M.F. Lemanski, F.C. Leitert, and C.G. Vinson, Catalyst and Process for Production of VCM, American Patent, Appl.4115323, 1978.
      [35]
      C. Liu and J.H. Lin, Influence of calcination temperature on dielectric constant and structure of the micro-crystalline muscovite, China Non-Metallic. Miner. Ind. Her., 2008, No. 5, p. 37.
      [36]
      Q.M. Wang, F.F. Jia, and S.X. Song, Study on effect of high temperature and ion exchange on crystal structure of natural muscovite, Non-Met. Mines, 39(2016), No. 1, p. 78.
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