Solid solution evolution during mechanical alloying in Cu-Nb-Al compounds

Kaouther Zaara; Mahmoud Chemingui; Virgil Optasanu; Mohamed Khitouni

doi:10.1007/s12613-019-1820-y

Volume 26 Issue 9

Sep. 2019

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文章导航 > 矿物冶金与材料学报（英文） > 2019 > 26(9): 1129-1139

Kaouther Zaara, Mahmoud Chemingui, Virgil Optasanu, and Mohamed Khitouni, Solid solution evolution during mechanical alloying in Cu-Nb-Al compounds, Int. J. Miner. Metall. Mater., 26(2019), No. 9, pp. 1129-1139. https://doi.org/10.1007/s12613-019-1820-y

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Kaouther Zaara, Mahmoud Chemingui, Virgil Optasanu, and Mohamed Khitouni, Solid solution evolution during mechanical alloying in Cu-Nb-Al compounds, Int. J. Miner. Metall. Mater., 26(2019), No. 9, pp. 1129-1139. https://doi.org/10.1007/s12613-019-1820-y

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Solid solution evolution during mechanical alloying in Cu-Nb-Al compounds

Laboratory of Inorganic Chemistry, UR 11-ES-73, University of Sfax, B. P. 1171, Sfax 3018, Tunisia
ICB, UMR 6303 CNRS, University of Bourgogne Franche Comté, 9 av. Alain Savary, 21078 Dijon Cedex, France

通讯作者:
Virgil Optasanu E-mail: virgil.optasanu@u-bourgogne.fr

中文摘要

This work concerns the structural evolution of Cu₇₀Nb₂₀Al₁₀ (at%) alloy processed by mechanical alloying using a planetary ball mill in air atmosphere for different times (4 to 200 h). The morphological, structural, microstructural, and thermal behaviors of the alloy were investigated by scanning electron microscopy, energy-dispersive spectroscopy, X-ray diffraction, and differential scanning calorimetry. X-ray diffraction patterns were examined using the Rietveld refinement technique with the help of the MAUD software. A disordered FCC-Cu(Nb,Al) solid solution was formed after 8 h of milling. The crystallite size, microstrain, and lattice parameter were determined by the Rietveld method. With increasing milling time, the crystallite size of the final product-ternary-phase FCC-Cu(Nb,Al)-is refined to the nanometer scale, reaching 12 nm after 200 h. This crystallographic structure combines good mechanical strength and good ductility. An increase in microstrain and partial oxidation were also observed with increasing milling time.

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Solid solution evolution during mechanical alloying in Cu-Nb-Al compounds

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Abstract

Abstract

This work concerns the structural evolution of Cu₇₀Nb₂₀Al₁₀ (at%) alloy processed by mechanical alloying using a planetary ball mill in air atmosphere for different times (4 to 200 h). The morphological, structural, microstructural, and thermal behaviors of the alloy were investigated by scanning electron microscopy, energy-dispersive spectroscopy, X-ray diffraction, and differential scanning calorimetry. X-ray diffraction patterns were examined using the Rietveld refinement technique with the help of the MAUD software. A disordered FCC-Cu(Nb,Al) solid solution was formed after 8 h of milling. The crystallite size, microstrain, and lattice parameter were determined by the Rietveld method. With increasing milling time, the crystallite size of the final product-ternary-phase FCC-Cu(Nb,Al)-is refined to the nanometer scale, reaching 12 nm after 200 h. This crystallographic structure combines good mechanical strength and good ductility. An increase in microstrain and partial oxidation were also observed with increasing milling time.
- powder metallurgy;
- mechanical alloying;
- nanomaterials;
- copper-based alloy;
- solid solution

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Solid solution evolution during mechanical alloying in Cu-Nb-Al compounds

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Solid solution evolution during mechanical alloying in Cu-Nb-Al compounds

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