2-巯基苯并噻唑浓度对API X60管线钢酸蚀行为的影响：电化学参数及吸附机理

Masoud Sabzi; Amir Hayati Jozani; Farzad Zeidvandi; Majid Sadeghi; Saeid Mersagh Dezfuli

doi:10.1007/s12613-020-2156-3

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文章导航 > 矿物冶金与材料学报（英文） > 2022 > 29(2): 271-282

Masoud Sabzi, Amir Hayati Jozani, Farzad Zeidvandi, Majid Sadeghi, and Saeid Mersagh Dezfuli, Effect of 2-mercaptobenzothiazole concentration on sour-corrosion behavior of API X60 pipeline steel: Electrochemical parameters and adsorption mechanism, Int. J. Miner. Metall. Mater., 29(2022), No. 2, pp. 271-282. https://doi.org/10.1007/s12613-020-2156-3

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Masoud Sabzi, Amir Hayati Jozani, Farzad Zeidvandi, Majid Sadeghi, and Saeid Mersagh Dezfuli, Effect of 2-mercaptobenzothiazole concentration on sour-corrosion behavior of API X60 pipeline steel: Electrochemical parameters and adsorption mechanism, Int. J. Miner. Metall. Mater., 29(2022), No. 2, pp. 271-282. https://doi.org/10.1007/s12613-020-2156-3

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2-巯基苯并噻唑浓度对API X60管线钢酸蚀行为的影响：电化学参数及吸附机理

1)
Young Researchers and Elite Club, Dezful Branch, Islamic Azad University, Dezful, Iran
2)
‎Department of Materials Science and Engineering, Science and Research Branch, Islamic Azad University, Tehran, ‎Iran
3)
Center of Excellence for Surface Engineering and Corrosion Protection of Industrial, School of Metallurgy and Materials Engineering, College of Engineering, University of Tehran, P.O. Box 11155-4563, Tehran, Iran

通讯作者:
Masoud Sabzi E-mail: mas.metallurg88@gmail.com

中文摘要

我们研究了2-巯基苯并噻唑浓度对API X60管线钢在25°C含H₂S环境中和0、2.5、5.0、7.5和10.0 g/L的2-巯基苯并噻唑抑制剂条件下的酸腐蚀行为的影响。我们利用开路电位 (OCP)、动电位极化和电化学阻抗谱(EIS)测试来研究这种腐蚀行为，利用能量色散光谱和扫描电子显微镜来分析腐蚀产物。OCP 和动电位极化测试结果表明，2-巯基苯并噻唑降低了阳极和阴极的反应速度。关于抑制剂的吉布斯自由能的评估表明其值在−20 kJ·mol⁻¹和−40 kJ·mol⁻¹之间。因此，2-巯基苯并噻唑对API X60管线钢表面的吸附既是物理也是化学吸附，其中后者是自发的。此外，由于吉布斯自由能值为负，我们可以得出结论，2-巯基苯并噻唑在管线钢表面的吸附是自发发生的。EIS结果表明，随着2-巯基苯并噻唑抑制剂浓度的增加，API X60钢的耐腐蚀性能提高。对腐蚀产物的分析表明，其表面形成了硫化铁化合物。总之，结果表明，缓蚀剂浓度的增加导致腐蚀速率的降低和缓蚀效率的增加。此外，我们发现在含H₂S的环境中API X60钢表面上的2-巯基苯并噻唑吸附行为遵循Langmuir吸附等温线并自发发生。

关键词:

Research Article

Effect of 2-mercaptobenzothiazole concentration on sour-corrosion behavior of API X60 pipeline steel: Electrochemical parameters and adsorption mechanism

+ Author Affiliations

Abstract

Abstract

We investigated the effect of ‎the 2-mercaptobenzothiazole concentration on the sour-corrosion behavior of API ‎X60 pipeline steel in an environment containing H₂S at 25°C and in the presence of 0, 2.5, 5.0, 7.5, and 10.0 g/L of ‎2-mercaptobenzothiazole inhibitor. To examine this behavior, we conducted open-circuit potential (OCP), potentiodynamic polarization, and electrochemical impedance spectroscopy (EIS) tests. Energy dispersive spectroscopy and scanning electron microscopy were also used to analyze the corrosion products. The results of the OCP and potentiodynamic polarization tests revealed that ‎2-mercaptobenzothiazole reduces the speed of both the anodic and cathodic reactions. An assessment of the Gibbs free energy of the inhibitor (
$ {\Delta G}_{\mathrm{a}\mathrm{d}\mathrm{s}}^{\ominus} $
) indicated that its value was less than −20 kJ·mol⁻¹ and greater than −40 kJ·mol⁻¹. Therefore, the adsorption of 2-mercaptobenzothiazole onto the surface of the API X60 pipeline steel occurs both physically and chemically, the latter of which is particularly intentional. In addition, as the
$ {\Delta G}_{\mathrm{a}\mathrm{d}\mathrm{s}}^{\ominus} $
value was negative, we could conclude that the adsorption of 2-mercaptobenzothiazole onto the surface of the pipeline steel occurs spontaneously. The EIS results indicate that with the increase in the 2-mercaptobenzothiazole inhibitor concentration, the corrosion resistance of API X60 steel increases. An analysis of the corrosion products revealed that iron sulfide compounds form on the surface. In summary, the results showed that an increase in the inhibitor concentration results in a decrease in the corrosion rate and an increase in inhibitory efficiency. Additionally, we found that the 2-mercaptobenzothiazole adsorption process on the API X60 steel surfaces in an H₂S-containing environment follows the Langmuir adsorption isotherm and occurs spontaneously.
- API X60 steel;
- sour corrosion;
- 2-mercaptobenzothiazole;
- inhibitor concentration;
- electrochemical parameters;
- environments containing hydrogen sulfide

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2-巯基苯并噻唑浓度对API X60管线钢酸蚀行为的影响：电化学参数及吸附机理

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Effect of 2-mercaptobenzothiazole concentration on sour-corrosion behavior of API X60 pipeline steel: Electrochemical parameters and adsorption mechanism

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