| Cite this article as: |
Yahya Jafari Tarzanagh, Davod Seifzadeh, and Roghaye Samadianfard, Combining the 8-hydroxyquinoline intercalated layered double hydroxide film and sol–gel coating for active corrosion protection of the magnesium alloy, Int. J. Miner. Metall. Mater., 29(2022), No. 3, pp. 536-546. https://doi.org/10.1007/s12613-021-2251-0
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Davod Seifzadeh E-mail: seifzadeh@uma.ac.ir
采用8-羟基喹啉（8-HQ）插层双氢氧化物（LDH）膜为底层和溶胶–凝胶层相结合的方法，对AM60B镁合金进行了腐蚀防护性能的研究。采用扫描电子显微镜（SEM）、场发射扫描电子显微镜（FESEM）、能量色散X射线能谱（EDS）、X射线衍射（XRD）、原子力显微镜（AFM）和电化学阻抗谱（EIS）等方法对LDH、LDH/溶胶–凝胶和LDH@HQ/溶胶–凝胶涂层进行分析。SEM图像显示，垂直生长的纳米片组成的LDH膜完全覆盖在表面。LDH/溶胶–凝胶和LDH@HQ/溶胶–凝胶涂层的形貌相同。此外，除了LDH@HQ/溶胶–凝胶涂层具有相对较高的表面粗糙度外，两种复合涂层的形貌几乎相同。虽然在3.5wt% NaCl溶液中，LDH膜具有与合金样品相同的阻抗行为，但其耐蚀性要高得多，这可能是由于其阻隔性以及对氯离子的捕获。与LDH薄膜相似，随着暴露时间的延长，LDH/溶胶–凝胶复合材料的耐蚀性降低。但其值远高于LDH膜，这主要与溶液路径的封闭有关。LDH@HQ/溶胶–凝胶复合材料的抗腐蚀性能优于LDH/溶胶–凝胶涂层，原因是8-HQ通过络合作用吸附在损伤部位。
8-hydroxyquinoline (8-HQ) intercalated layered double hydroxides (LDH) film as underlayer and sol–gel layer was combined for active corrosion protection of the AM60B magnesium alloy. The LDH, LDH/sol–gel, and LDH@HQ/sol–gel coatings were analyzed using the scanning electron microscopy (SEM), field emission scanning electron microscopy (FESEM), energy dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD), atomic force microscopy (AFM), and electrochemical impedance spectroscopy (EIS) methods. The SEM images showed that the surface was entirely coated by the LDH film composed of vertically-grown nanosheets. The same morphology was observed for the LDH/sol–gel and LDH@HQ/sol–gel coatings. Also, almost the same topography was observed for both composite coatings except that the LDH@HQ/sol–gel coating had relatively higher surface roughness. Although the LDH film had the same impedance behavior as the alloy sample in 3.5wt% NaCl solution, its corrosion resistance was much higher, which could be due to its barrier properties as well as to the trapping of the chloride ions. Similar to the LDH film, the corrosion resistance of the LDH/sol–gel composite diminished with increasing the exposure time. However, its values were much higher than that of the LDH film, which was mainly related to the sealing of the solution pathways. The LDH@HQ/sol–gel composite showed much better anti-corrosion properties than the LDH/sol–gel coating due to the adsorption of the 8-HQ on the damaged areas through the complexation.
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