高性能NiCoZn/C@海绵衍生碳复合吸波材料

解秀波; 王河山; 木村秀夫; 倪翠; 杜伟; 吴广磊

doi:10.1007/s12613-024-2880-1

Volume 31 Issue 10

Oct. 2024

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文章导航 > 矿物冶金与材料学报（英文） > 2024 > 31(10): 2274-2286

Xiubo Xie, Heshan Wang, Hideo Kimura, Cui Ni, Wei Du, and Guanglei Wu, NiCoZn/C@melamine sponge-derived carbon composites with high-performance electromagnetic wave absorption, Int. J. Miner. Metall. Mater., 31(2024), No. 10, pp. 2274-2286. https://doi.org/10.1007/s12613-024-2880-1

Cite this article as:

Xiubo Xie, Heshan Wang, Hideo Kimura, Cui Ni, Wei Du, and Guanglei Wu, NiCoZn/C@melamine sponge-derived carbon composites with high-performance electromagnetic wave absorption, Int. J. Miner. Metall. Mater., 31(2024), No. 10, pp. 2274-2286. https://doi.org/10.1007/s12613-024-2880-1

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研究论文

高性能NiCoZn/C@海绵衍生碳复合吸波材料

1)
烟台大学环境与材料工程学院, 烟台 264005, 中国
2)
山东航空学院山东省黄河三角洲生态环境科学重点实验室, 滨州 256603, 中国
3)
青岛大学材料科学与工程学院能源与环境材料研究院, 青岛 266071, 中国

通讯作者:
解秀波    E-mail: xiuboxie@ytu.edu.cn

杜伟    E-mail: duwei@ytu.edu.cn

吴广磊    E-mail: wuguanglei@qdu.edu.cn

文章亮点

(1) 系统地研究了元素替换对Ni₃ZnC_0.7/海绵衍生碳材料物相及形貌的影响规律

(2) Co、Fe和Mn中Co元素对碳纳米管生成促进作用最明显

(3) 总结了NiCoZn/C@海绵衍生碳材料的吸波机理

中文摘要

开发高性能吸波材料是解决电磁污染的重要途径。本文为了降低复合材料的密度并明确Co、Fe和Mn元素对NiMZn/C@海绵衍生碳(MSDC)复合材料物相及形貌的影响，通过真空抽滤和真空煅烧法制备了NiMZn/C@海绵衍生碳复合材料。在NiCoZn/C@MSDC复合材料中，大量碳纳米管(CNTs)均匀附着在三维交联的海绵状碳的表面，在NiFeZn/C@MSDC和NiMnZn/C@MSDC复合材料中也检测到碳纳米管。NiFeZn/C@MSDC和NiMnZn/C@MSDC复合材料中均发现原位生成的Ni₃ZnC_0.7、Ni₃Fe和MnO物相。原位生成的碳纳米管有效调控了复介电常数。NiCoZn/C@海绵衍生碳复合材料具有最优的性能：在匹配厚度为1.4mm时最低反射损失值为−33.1 dB；在匹配厚度为1.7mm时吸收带宽为5.04 GHz。良好的阻抗匹配，优异的界面极化及偶极子极化，高导电损耗及多重反射/散射效应提高了复合材料的吸波性能。

关键词:

Research Article

NiCoZn/C@melamine sponge-derived carbon composites with high-performance electromagnetic wave absorption

+ Author Affiliations

1)
School of Environmental and Material Engineering, Yantai University, Yantai 264005, China
2)
Shandong Key Laboratory of Eco-Environmental Science for the Yellow River Delta, Shandong University of Aeronautics, Binzhou 256603, China
3)
Institute of Materials for Energy and Environment, State Key Laboratory of Bio-fibers and Eco-textiles, College of Materials Science and Engineering, Qingdao University, Qingdao 266071, China

Guanglei Wu is an editorial board member for this journal and was not involved in the editorial review or the decision to publish this article. All authors declare no financial/commercial conflicts of interest.

Corresponding authors:
Xiubo Xie    E-mail: xiuboxie@ytu.edu.cn

Wei Du    E-mail: duwei@ytu.edu.cn

Guanglei Wu    E-mail: wuguanglei@qdu.edu.cn
Received: 15 January 2024; Revised: 8 March 2024; Accepted: 11 March 2024; Available online: 13 March 2024

Abstract

Abstract

NiMZn/C@melamine sponge-derived carbon (MSDC) composites (M = Co, Fe, and Mn) were prepared by a vacuum pumping solution method followed by carbonization. A large number of carbon nanotubes (CNTs) homogeneously attached to the surfaces of the three-dimensional cross-linked of the sponge-derived carbon in the NiCoZn/C@MSDC composite, and CNTs were detected in the NiFeZn/C@MSDC and NiMnZn/C@MSDC composites. Ni₃ZnC_0.7, Ni₃Fe, and MnO in-situ formed in the NiFeZn/C@MSDC and NiMnZn/C@MSDC composites. The CNTs in the NiCoZn/C@MSDC composite efficiently modulated its complex permittivity. Thus, the composite exhibited the best performance among the composites, with the minimum reflection loss (RL_min) of −33.1 dB at 18 GHz and thickness of 1.4 mm. The bandwidth for RL of ≤−10 dB was up to 5.04 GHz at the thickness of 1.7 mm and loading of 25wt%. The optimized impedance matching, enhanced interfacial and dipole polarization, remarkable conduction loss, and multiple reflections and scattering of the incident microwaves improved the microwave absorption performance. The effects of Co, Ni, and Fe on the phase and morphology provided an alternative way for developing highly efficient and broadband microwave absorbers.
- microwave absorption;
- carbon nanotube;
- element substitution;
- melamine sponge-derived carbon

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