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Roughness characterization and shearing dislocation failure for rock–backfill interface

Meifeng Cai, Zhilou Feng, Qifeng Guo, Xiong Yin, Minghui Ma, Xun Xi

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Cite this article as:

Meifeng Cai, Zhilou Feng, Qifeng Guo, Xiong Yin, Minghui Ma, and Xun Xi, Roughness characterization and shearing dislocation failure for rock–backfill interface, Int. J. Miner. Metall. Mater., 31(2024), No. 6, pp.1167-1176. https://dx.doi.org/10.1007/s12613-024-2901-0
Meifeng Cai, Zhilou Feng, Qifeng Guo, Xiong Yin, Minghui Ma, and Xun Xi, Roughness characterization and shearing dislocation failure for rock–backfill interface, Int. J. Miner. Metall. Mater., 31(2024), No. 6, pp.1167-1176. https://dx.doi.org/10.1007/s12613-024-2901-0
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研究论文

围岩–充填体界面粗糙度表征与剪切错动破坏研究

    通信作者:

    郭奇峰 E-mail: guoqifeng@ustb.edu.cn

文章亮点

(1) 设计了考虑节理形貌粗糙系数的围岩-充填体剪切错动试验方法 (2) 得到了围岩–充填体界面的三维分形维数、剖面线二维分形维数和表面曲率 (3) 揭示了围岩–充填体界面剪切错动力学行为和破坏特征
金属矿充填开采过程中,充填体沉降或采掘扰动作用下,围岩与充填体界面存在剪切错动,影响采场稳定性。本文设计了围岩-充填体剪切错动试验方法,结合数字图像技术与三维激光形貌扫描技术,建立了一套粗糙节理面三维建模流程,基于剪切试验探究了基于自由节理面的围岩-充填体组合体剪切错动力学行为及破坏特征。提出的建模分析方法可获得粗糙面的三维分形维数、剖面线JRC均值、剖面线二维分形维数均值和断裂面表面曲率,通过相关性分析能够实现表面粗糙度的关联表征,进而通过JRC测算剪切强度。试验剪切破坏特征显示:组合体剪切错动有3个破坏阈值点,分别位于峰前段位移30%–50%、峰前段位移70%–90%和峰前段位移100%后,可作为围岩充填体错动破坏判别的征兆;通过围岩表面JRC可判断围岩与充填体剪切错动峰后滑移、均匀变化、阶梯变化的类型,对应工程现场的围岩充填体错动破坏过程类型。该研究揭示了基于自由节理面的异构组合体力学损伤机制,弥补了现有含粗糙节理异构组合体剪切理论体系的不足,为防治矿山充填灾害提供了理论依据。

 

Research Article

Roughness characterization and shearing dislocation failure for rock–backfill interface

Author Affilications
    Corresponding author:

    Qifeng Guo      E-mail: guoqifeng@ustb.edu.cn

  • Received: 09 March 2024; Revised: 31 March 2024; Accepted: 01 April 2024; Available online: 02 April 2024
Shearing dislocation is a common failure type for rock–backfill interfaces because of backfill sedimentation and rock strata movement in backfill mining goaf. This paper designed a test method for rock–backfill shearing dislocation. Using digital image technology and three-dimensional (3D) laser morphology scanning techniques, a set of 3D models with rough joint surfaces was established. Further, the mechanical behavior of rock–backfill shearing dislocation was investigated using a direct shear test. The effects of interface roughness on the shear–displacement curve and failure characteristics of rock–backfill specimens were considered. The 3D fractal dimension, profile line joint roughness coefficient (JRC), profile line two-dimensional fractal dimension, and the surface curvature of the fractures were obtained. The correlation characterization of surface roughness was then analyzed, and the shear strength could be measured and calculated using JRC. The results showed the following: there were three failure threshold value points in rock–backfill shearing dislocation: 30%–50% displacement before the peak, 70%–90% displacement before the peak, and 100% displacement before the peak to post-peak, which could be a sign for rock–backfill shearing dislocation failure. The surface JRC could be used to judge the rock–backfill shearing dislocation failure, including post-peak sliding, uniform variations, and gradient change, corresponding to rock–backfill dislocation failure on the field site. The research reveals the damage mechanism for rock–backfill complexes based on the free joint surface, fills the gap of existing shearing theoretical systems for isomerism complexes, and provides a theoretical basis for the prevention and control of possible disasters in backfill mining.

 

  • Due to the requirements for green mine construction, the backfill mining method has been widely adopted in underground mines [13]. Because the backfill close to the roof is imperfect, the backfill support for the roof in the space area is limited, and its role is mainly to restrict the lateral deformation of surrounding rock and vertical dislocation during the self-sedimentation of backfill or deformation of surrounding rock. Therefore, the shearing properties of the interfaces between surrounding rocks and backfills significantly affect the stability of backfilled mining goaf [45].

    In the past decades, considerable research has been conducted on backfill mixtures and mechanical properties [67]. For instance, Wu et al. [8] developed a low-alkalinity activation method to improve the mechanical performance of cemented rockfill. Meanwhile, a strength prediction model considering the material, ultrasonic, and stress properties of cemented waste rock–backfill for recycling gangue was developed by Wu et al. [9]. Zhao et al. [10] investigated the effects of water content, water type, and temperature on the rheological behavior of slag–cement and fly ash–cement paste backfill. Wang et al. [11] conducted triaxial cyclic loading and unloading tests to study the mechanical properties and microstructure of layered cemented paste backfill and found that a large number of pores existed in the post-filling layer, which was compacted at early cycles. However, the stability of backfill mining goaf is dependent not only on the properties of the backfill but also on the coupling properties of rock–backfill combination structures.

    Indeed, many rock projects involve the mechanics of combined rock strata. In this regard, Xie et al. [12] analyzed the influence of surface roughness on the mechanical properties of the combination of dam body and dam foundation. Liu et al. [13] studied the shearing failures of combined rock and concrete through direct shearing numerical simulations. Yi et al. [1415] investigated the effects of static load strength, cohesive force, fracture toughness ratio, volume ratio, and interface roughness on the mechanical properties of combined models. The coupling mechanical response of dam bodies and dam foundations at an engineering scale also have been investigated [1617]. Zuo et al. [1819] focused the damage mechanism for the compressive deformation of coal and rock complexes and proposed a nonlinear model for their failure. Meanwhile, Li et al. [2021] studied the failure process of coal and rock complexes and fractal features from the perspective of impact load and revealed the cooperation mechanism of coal and rock complexes under the action of dynamic disturbance. Chen et al. [22] analyzed the influence of coal and rock combination ratios on strength, elastic modulus, and strength before the peak and proposed mechanical models and judgment mechanisms for buckling failure of coal and rock complexes. Yang et al. [23] conducted compression tests and numerical simulations considering interfaces and revealed the influencing mechanism of interfaces on the destruction and evolutionary process of complexes.

    Existing research on different combinations of rock, concrete, and coal, among others, proves that interfaces play a significant role in the failure of such combinations. However, rock interfaces are normally rough, and the effect of interface roughness on rock–backfill shearing failure has rarely been considered. Thus, this paper took a small unit of surrounding rock and backfill shown in Fig. 1 as the research object and designed shear tests for rock–backfill combinations to investigate the influence of rough joint surfaces on shearing dislocation failure between backfill and surrounding rock, thus guiding the design of backfill mining.

    Figure  1.  Diagram for filling in the space area.

    Granite is one of the most common rock types in hard-rock mines. To investigate the failure of shearing dislocation between the backfill and surrounding rock based on a free fracture surface, a granite rock beam was broken into a fracture surface with realistic roughness based on the three-point beam bending test and then placed in the mold with the backfill to make a rock–backfill combination for direct shear tests.

    After a granite beam of 100 mm × 100 mm × 30 mm was broken through a three-point beam bending test, the surface morphology of the fracture surface was obtained. Then, the granite specimen was placed in a mold, and the backfill was mixed and poured with the granite. The water content of the backfill was 25wt%, and the weight ratio of cement bindings to tailings was 1:3. The rock–backfill combination was demolded after 48 h under an indoor environment and then put into a standard curing box for 28 d. Fig. 2 shows an example of the final specimen.

    Figure  2.  Rock–backfill specimen.

    A Talysurf CLI2000 three-dimensional (3D) laser morphology scanner was used to conduct the overall scanning and modeling for the fracture surface of the granite. 3D data of the fracture surface were imported as 3D surface cloud pictures into software to quantify surface roughness.

    A direct shearing device was used to conduct shear tests for the rock–backfill combination, and a digital image correlation (DIC) device was used to monitor the shearing failure process to study the failure for shearing dislocation between the backfill and the surrounding rock. The rock–backfill shear test was conducted using the rock shearing testing machine (TFD-20H/50J) produced by Changchun Keyi Test Instrument Co., Ltd. The normal peak load was 20 kN, and the tangential peak load was 50 kN. During the shearing process, a displacement control method was used. The shearing rate was 0.1 mm/min. A StrainMaster Portable strain measurement system (DIC devices) produced by LaVision in Germany was used to conduct real-time monitoring for the surface deformation of test specimens and record the shearing deformation process of complex specimens. The test system was arranged as shown in Fig. 3.

    Figure  3.  Photograph of test system.

    JRC is an important parameter that measures the roughness of a joint. It is also one of the important factors that affect the mechanical behavior of rock–backfill specimens. For the rock–backfill combination, the interface between the rock and the backfill was dependent on the surface of the rock, which could be characterized by JRC. Joint surfaces are generally random and ruleless. Thus, describing roughness through quantification is of great significance. At the earliest, Barton and Choubey [24] put forward a concept for describing the roughness degree of a structural surface with JRC through tests and gave 10 typical roughness joints where JRC ranged from 0 to 20 in 1976. For an unknown curve, we can compare it with the Barton standard curve to get its JRC.

    Mandelbrot [25] created fractal geometry theory in 1967, which was first introduced by Turk et al. [26] to JRC research in 1987, and the quantitative relation between fractal dimension and JRC was established thereby. Fractal is a collection of similar bodies; the joint hatching line has overall similarity, and the up-and-down details are of statistical significance and meet the definition of fractal. Therefore, the fractal theory’s advantages of being used for joint roughness are congenital.

    Ten Barton standard curves put forward by Barton did not give a definite JRC value. The relational expression of JRC and fractal dimension established by Xie [27] is one of the methods that are widely used to calculate JRC based on fractal dimension at present.

    This paper chose the box fractal dimension method to measure the fractal dimension value of different Barton curves and completed the quantification of JRC based on Eq. (1).

    JRC=85.2671(D1)0.5679 (1)

    where D represents fractal dimention.

    The box fractal dimension method [28] uses grids with a side length of δ to cover the figure that must be measured and calculates the number of boxes required to cover the whole figure. The side length of boxes must be continuously reduced to obtain the number of boxes required to cover the figure under different side lengths. Using the equation for box fractal dimension, the special box fractal dimension is obtained, and two-dimensional boxes are changed to three-dimensional cubes. The method can be mapped to three-dimensional figures.

    After the granite rock beam was broken through the three-point bending test, a 3D laser morphology scanner was used to conduct overall scanning for the fracture bodies of the granite to obtain a 3D cloud picture. Only the 3D fracture bodies near the fracture surface were related to the roughness of the fracture surface. Therefore, a 3D surface cloud picture was used to characterize the surface roughness. The specific process is as follows:

    (1) Define the coordinates of the 3D surface cloud picture again and generate a new entity coordinate system.

    (2) Convert the 3D surface cloud picture into a 3D entity to facilitate subsequent section and operation. The digital scanning surface cloud picture before conversion is shown in Fig. 4(a), and the entity picture after conversion is shown in Fig. 4(b).

    Figure  4.  Process for extracting fracture bodies: (a) digital scanning surface cloud picture; (b) volume rendering entity picture; (c) zone of fracture.

    (3) Position the wave crest and trough of the fracture surface through a section and cut off the area outside the zone of fracture according to the coordinates of the crest and trough to generate the new entity of the zone of fracture, as shown in Fig. 4(c).

    (4) Complete the section, calculation of fractal dimension, curvature, and other parameters, data export, and other subsequent operations on the new entity of the zone of fracture.

    The roughness parameters of fracture bodies include the three-dimensional fractal dimension, two-dimensional profile fractal dimension, JRC, and surface curvature of the fracture surface. The method of calculating them is as follows:

    (1) Three-dimensional fractal dimension.

    Based on an unfixed boundary, this is calculated using the box fractal dimension method shown in Eq. (2):

    DB=lim (2)

    where DB refers to the box fractal dimension, δ refers to the side length of the grid cover mass, F refers to the fractal set, and Nδ(F) refers to the number of boxes.

    (2) Two-dimensional profile fractal dimension.

    Using the box fractal dimension method shown in Eq. (2), the specimen was divided into a two-dimensional section to calculate the box fractal dimension of a two-dimensional profile and the mean value. The typical profile during the computational process is shown in Fig. 5.

    Figure  5.  Typical profile maps in calculating the profile fractal dimension: (a) map 1; (b) map 2; (c) map 3.

    (3) JRC.

    To calculate JRC according to the two-dimensional profile fractal dimension, take specimen 1-1 as the object and select 20 profiles with equal spacing. First, demarcate the JRC of 20 profiles according to the Barton standard curve. Then, calculate the two-dimensional fractal dimension of all profiles. Afterward, based on Eq. (1) fitting, obtain the relationship between the fractal dimension of specimen 1-1 and JRC, as shown in Eq. (3). Lastly, calculate the JRC of all profiles according to Eq. (3) and the mean value.

    {\text{JRC}} = 21.07{\left( {D - 1} \right)^{0.49}} (3)

    (4) Surface curvature.

    The Generate Surface command was used to generate a surface cloud picture of fracture bodies. The Curvature and Surface View commands were used to view the surface curvature of the fracture surface, whereas the Histogram command was used to view the value of the surface curvature.

    The result of calculating the 3D fractal dimension of fracture bodies, profile line JRC mean value, profile line two-dimensional fractal dimension mean value, and surface curvature of the fracture surface with the above methods are shown in Table 1. The 3D fractal dimension of fracture bodies, profile line JRC mean value, and profile line two-dimensional fractal dimension mean value had a good consistency. The JRC of fracture bodies ranged from 12 to 18, consistent with those calculated using the Barton standard curve during a preliminary study [29]. The surface curvature of the fracture surface was weak compared with other parameters.

    Table  1.  JRC of the free fracture surface, fractal dimension, and surface curvature
    No. 3D fractal dimension of
    fracture bodies
    Profile line JRC
    mean value
    Profile line two-dimensional fractal dimension mean value Surface curvature of the fracture surface
    1-1 2.564 15.862 1.564 2.001
    1-2 2.528 16.466 1.609 1.961
    2-1 2.400 13.826 1.426 1.960
    2-2 2.560 15.548 1.543 2.064
    3-1 2.354 13.229 1.389 1.151
    3-2 2.560 16.414 1.603 2.046
    4-1 2.441 15.816 1.559 2.401
    4-2 2.495 15.234 1.523 2.030
    5-1 2.432 15.053 1.507 2.641
    5-2 2.427 14.957 1.504 2.248
    6-1 2.495 14.621 1.483 2.117
    6-2 2.332 13.719 1.420 0.721
    7-1 2.498 16.070 1.577 1.699
    7-2 2.491 14.878 1.497 2.199
    8-1 2.511 14.984 1.507 1.587
    8-2 2.319 12.835 1.367 1.191
    下载: 导出CSV 
    | 显示表格

    The surface curvature plot of the fracture surface generated by 16 specimens and the fracture surface under volume rendering are shown in Fig. 6. The middle-upper part of each specimen drawing belonged to the fracture surface of rendering, whereas the lower part was the surface curvature plot of the fracture surface. The colors show the differences in the surface curvature. The closer the color to red, the larger the surface curvature.

    Figure  6.  Surface curvature of the fracture surface: (a) specimen 1-1; (b) specimen 1-2;(c) specimen 2-1; (d) specimen 2-2; (e) specimen 3-1; (f) specimen 3-2; (g) specimen 4-1; (h) specimen 4-2; (i) specimen 5-1; (j) specimen 5-2; (k) specimen 6-1; (l) specimen 6-2; (m) specimen 7-1; (n) specimen 7-2; (o) specimen 8-1; (p) specimen 8-2.

    Fig. 6 shows that JRC matched the surface curvature relatively. Taking specimens 1-1, 1-2, 2-1, and 2-2 as examples, specimen 1-2 had a wide red area and large quantity, corresponding to the maximum JRC; meanwhile, specimen 2-1 had a narrow red area and small quantity, corresponding to the minimum JRC. However, as far as some specimens were concerned, the surface curvature was not consistent with JRC, indicating that measuring the applicability of JRC with surface curvature had limitations to a certain extent.

    Fig. 7 shows the relationship between JRC and the mean fractal dimension of a profile. Both had extremely good index-fitting relationships, as shown in Eq. (4). The coefficient of determination is 0.999.

    Figure  7.  Relationship between JRC and the mean fractal dimension of a profile.
    {\text{JRC}} = 43.278 \times {D^{0.434}} - 36.688 (4)

    The fitting equation provides new thought for JRC calculation. JRC can be calculated directly after the two-dimensional fractal dimension mean value is obtained, which is a more convenient way for calculating the mean value compared with Eq. (3) requiring JRC calculation first.

    Fig. 8 shows the relationship between the fractal dimension of fracture bodies and the mean fractal dimension of the profile. Both had good linear growth relationships. The linear fitting relationship is shown in Eq. (5).

    Figure  8.  Relationship between the fractal dimension of fracture bodies and the mean fractal dimension of a profile
    y = 0.941x + 1.046 (5)

    Fig. 9 shows the relationship between JRC and the fractal dimension of fracture bodies. Both had good linear correlations as well. The linear fitting relationship is shown in Eq. (6), and the coefficient of determination is 0.736. The correlation between two-dimensional JRC was obtained according to the three-dimensional fractal dimension and profile line, and the three-dimensional fractal dimension could characterize the roughness of fracture bodies.

    Figure  9.  Relationship between JRC and the fractal dimension of fracture bodies.
    {\text{JRC}} = 11.757 \times D - 13.988 (6)

    Fig. 10 shows the relationship between shear strength τ and JRC. Both had quadratic function relationships, as shown in Eq. (7). The coefficient of determination is 0.968.

    Figure  10.  Relationship between shear strength and JRC.
    \tau=-0.002713\text{JR}\text{C}^{\text{2}}+0.227637\text{JRC}-1.49246 (7)

    where τ is the shear strength.

    Substituting Eq. (6) into Eq. (7), we can predict the shear strength with fracture dimension, and the expression is as follows:

    \begin{split} \tau= & -0.002713\times \left(11.757D-13.988\right)^2+0.227637\ \times \\ & \left(11.757D-13.988\right)-1.49246 \end{split} (8)

    With the value of the three-dimensional fracture dimension, we can obtain the calculated shear strength and actual shear strength using Eq. (8), as shown in Fig. 11. The error mean of both is 4.99%, indicating that Eq. (8) is relatively reliable and the shear strength and three-dimensional fracture dimension have a quadratic function relationship. With the increase in the three-dimensional fracture dimension, the shear strength also continues increasing, and the fundamental reason lies in the increase in the roughness.

    Figure  11.  Relationship between calculated shear strength and actual shear strength.

    Fig. 12 shows the rock–backfill shear stress–displacement curve of different specimens. JRC was from low to high. The shear stress–displacement curve entered a slip stage, uniform descent section, and stepwise descent section after a pear shear stress point was achieved. The JRC threshold values of the three curves were 12–14, 14–16, and 16–18, respectively. The different curve types mainly depended on the proportion of steep joint peaks and gentle joint peaks on the rough surface. The wear conditions of the interface from the backfill side were more significant than those from the rock side because the backfill was much weaker than the rock. Therefore, the rough joint was a key factor that decided the rock–backfill shear stress–displacement curve and JRC parameters that could be used for judging different curve types.

    Figure  12.  Rock–backfill shear stress–displacement curve: (a) specimen 3-1; (b) specimen 2-1;(c) specimen 7-2; (d) specimen 5-2; (e) specimen 1-2.

    Fig. 13 shows the strain field during typical rock–backfill failure. When there was a 10% displacement before the peak, there was a small range of displacement around the complex because of the boundary effect of the shear stress load. When there was a 30% displacement before the peak, the joint profile was shown on the strain cloud picture. When there was a 50% displacement before the peak, the shape change of the joint surface increased, and the peak strain value increased by 250% compared with that when there was a 30% displacement before the peak. When there was a 70% displacement before the peak, the complex profile had a shape change under the action of shear force. When there was a 90% displacement before the peak, the joint surface of the complex was damaged, and the joint surface slipped, resulting in the failure of the partial joint peak. When there was a 100% displacement before the peak, the partial joint peak had a brittle failure, and the joint surface could not be engaged. The strain cloud picture also had fault phenomena.

    Figure  13.  Rock–backfill failure at different displacements before the peak: (a) 10%; (b) 30%; (c) 50%; (d) 70%; (e) 90%; (f) 100%.

    Fig. 14 shows a simplified rock–backfill model. A small microbody in the interface of the backfill and granite was taken to conduct an analysis. During the shear test, there was fixed axial stress above, below, and on two sides of the complex to ensure that the shear test could be conducted normally. The stress refers to σ2 in the figure. The test system exerted shear force on the complex from right to left, and force was directly exerted on the backfill, forming σ1B. At this time, because of the counteracting force of the fixed bin, the granite also underwent σ1G rightward. Because the elasticity modulus of granite was larger than that of the backfill, the backfill produced external expansion failure before granite after being impacted by an external force. However, because of the cohesive force, the bonding surface exerted an inward restraining force, that is, σ3B, and it exerted a counteracting force σ3G on the granite at the same time. At this time, the backfill component was under compressive stress in three directions, whereas the granite was under a pulling-compressive stress state. According to the Griffith theory [30], the strength of the granite component close to the bonding surface is weaker than that of the granite in other parts and the strength of the backfill component is larger than the backfill in other parts.

    Figure  14.  Simplified rock–backfill model.

    With the boundary of the contact surface, the complex was divided into four parts: granite close to the bonding surface, granite away from the bonding surface, backfill close to the bonding surface, and backfill away from the bonding surface. For the granite, the strength of the granite away from the bonding surface was larger than that of the granite close to the bonding surface. For the backfill, the strength of the backfill close to the bonding surface was larger than that of the backfill away from the bonding surface. Typical rock–backfill DIC strain cloud pictures after the peak based on the free fracture surface of 16 specimens were selected, as shown in Fig. 15.

    Figure  15.  Rock–backfill failure after the peak of different specimen: (a) specimen 2-2; (b) specimen 3-1;(c) specimen 3-2; (d) specimen 4-1; (e) specimen 4-2; (f) specimen 5-1; (g) specimen 5-2; (h) specimen 6-2; (i) specimen 7-2; (j) specimen 8-1.

    After the peak, the granite close to the bonding surface showed obvious shape change and damage. The reason was that the fracture surface had many secondary microcracks after the granite was crushed through the bending test under three-point loading, resulting in low strength in the component of the granite close to the bonding surface. After being impacted by shear stress, the steep joint peak was stressed, which awakened the secondary cracks nearby, extended the connection, and produced the main defect surface until brittle failure.

    During actual engineering, after the surrounding rock in the stope undergoes external loading, such as drilling and blasting, the main defect surface causes the surrounding rock to fall and break and produces many secondary cracks near the defect surface. After the slurry is filled, the secondary cracks of the surrounding rock near the bonding surface still exist. Because of the acting force of the bonding surface and secondary cracks, the surrounding rock more easily undergoes brittle failure, resulting in potential hazards.

    The paper designed a rock–backfill shearing dislocation test method in combination with digital image technology and 3D laser morphology scanning technology. A set of 3D modeling processes with rough joint surfaces was established, and the mechanical behavior and failure of rock–backfill shearing dislocation based on the free joint surface were investigated. The main conclusions were drawn as follows:

    (1) The developed method of the rough joint surface in this paper can be used to obtain the 3D fractal dimension of a rough surface, profile line two-dimensional fractal dimension mean values, and the surface curvature of the fracture surface. The correlation characterization of surface roughness can be realized through correlation analysis.

    (2) The 3D fractal dimension of fracture bodies and profile line two-dimensional fractal dimension mean value had a good consistency. The relationship between the shear strength of the interface and the fractal dimensions was established.

    (3) The rock–backfill complex had three failure threshold value points in total, located in 30%–50% displacement before the peak, 70%–90% displacement before the peak, and 100% displacement before the peak to post-peak, respectively. The shear stress–displacement curve of the complex could be classified into three categories: slip, uniform descent, and stepwise descent after the peak.

    The shear dislocation of the rock–backfill interface was also affected by normal stress, which was not considered in the present work. Thus, the developed model for predicting interface shear dislocation needs to be improved by considering normal stress in future works.

    This work is supported by the National Key Research and Development Program of China (No. 2021YFC3001302) and the National Natural Science Foundation of China (No. 52274072).

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