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Volume 13 Issue 5
Oct.  2006
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Bing Su, Guoqing Zhang, Xudong Yu,  and Chengtao Wang, Sol-gel derived bioactive hydroxyapatite/titania composite films on Ti6Al4V, J. Univ. Sci. Technol. Beijing, 13(2006), No. 5, pp. 469-475. https://doi.org/10.1016/S1005-8850(06)60095-9
Cite this article as:
Bing Su, Guoqing Zhang, Xudong Yu,  and Chengtao Wang, Sol-gel derived bioactive hydroxyapatite/titania composite films on Ti6Al4V, J. Univ. Sci. Technol. Beijing, 13(2006), No. 5, pp. 469-475. https://doi.org/10.1016/S1005-8850(06)60095-9
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Materials

Sol-gel derived bioactive hydroxyapatite/titania composite films on Ti6Al4V

  • 通讯作者:

    Bing Su    E-mail: subing@sjtu.edu.cn

  • The composite films consisting of the titania gel impregnated with hydroxyapatite (HAP) submicron particles were prepared on commercial Ti6Al4V plates processed by a sol-gel route. HAP powders were synthesized based on wet chemical precipitation method with Ca(NO3)2·4H2O and (NH4)2HPO4 as starting reagents. After being calcined at 900°C,HAP powders were ultrasonically scattered in ethanol to produce HAP sol. The titania sol was prepared using titanium (IV) isopropoxide {Ti[OCH(CH3)2]4} as precursor. Both the titania sol and the HAP/titania mixture were sequentially spin-coated on the substrates and calcined at various temperatures. The characteristics and mechanical adhesion of the composite films were investigated. The results show that the as-prepared films are dense,homogeneous,well-crystallized,and there is a good interfacial adhesion between the film and the substrate. The in vitro bioac-tivities of these films were discussed based on the analysis of the variations of Ca and P concentrations in the simulated body fluid and their surface morphologies against immersion time.
  • Materials

    Sol-gel derived bioactive hydroxyapatite/titania composite films on Ti6Al4V

    + Author Affiliations
    • The composite films consisting of the titania gel impregnated with hydroxyapatite (HAP) submicron particles were prepared on commercial Ti6Al4V plates processed by a sol-gel route. HAP powders were synthesized based on wet chemical precipitation method with Ca(NO3)2·4H2O and (NH4)2HPO4 as starting reagents. After being calcined at 900°C,HAP powders were ultrasonically scattered in ethanol to produce HAP sol. The titania sol was prepared using titanium (IV) isopropoxide {Ti[OCH(CH3)2]4} as precursor. Both the titania sol and the HAP/titania mixture were sequentially spin-coated on the substrates and calcined at various temperatures. The characteristics and mechanical adhesion of the composite films were investigated. The results show that the as-prepared films are dense,homogeneous,well-crystallized,and there is a good interfacial adhesion between the film and the substrate. The in vitro bioac-tivities of these films were discussed based on the analysis of the variations of Ca and P concentrations in the simulated body fluid and their surface morphologies against immersion time.
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