Hui-bin Wu, Gang Niu, Feng-juan Wu, and Di Tang, Reverse-transformation austenite structure control with micro/nanometer size, Int. J. Miner. Metall. Mater., 24(2017), No. 5, pp. 530-537. https://doi.org/10.1007/s12613-017-1434-1
Cite this article as:
Hui-bin Wu, Gang Niu, Feng-juan Wu, and Di Tang, Reverse-transformation austenite structure control with micro/nanometer size, Int. J. Miner. Metall. Mater., 24(2017), No. 5, pp. 530-537. https://doi.org/10.1007/s12613-017-1434-1
Research ArticleOpen Access

Reverse-transformation austenite structure control with micro/nanometer size

+ Author Affiliations
  • Corresponding author:

    Gang Niu    E-mail: ustbning@163.com

  • Received: 1 September 2016Revised: 13 December 2016Accepted: 14 December 2016
  • To control the reverse-transformation austenite structure through manipulation of the micro/nanometer grain structure, the influences of cold deformation and annealing parameters on the microstructure evolution and mechanical properties of 316L austenitic stainless steel were investigated. The samples were first cold-rolled, and then samples deformed to different extents were annealed at different temperatures. The microstructure evolutions were analyzed by optical microscopy, scanning electron microscopy (SEM), magnetic measurements, and X-ray diffraction (XRD); the mechanical properties are also determined by tensile tests. The results showed that the fraction of stain-induced martensite was approximately 72% in the 90% cold-rolled steel. The micro/nanometric microstructure was obtained after reversion annealing at 820-870℃ for 60 s. Nearly 100% reversed austenite was obtained in samples annealed at 850℃, where grains with a diameter ≤ 500 nm accounted for 30% and those with a diameter >0.5 μm accounted for 70%. The micro/nanometer-grain steel exhibited not only a high strength level (approximately 959 MPa) but also a desirable elongation of approximately 45%.
  • loading
  • [1]
    R.D.K. Misra, W.W. Thein-Han, T.C. Pesacreta, M.C. Somani, and L.P. Karjalainen, Biological significance of nanograined/ultrafine-grained structures:Interaction with fibroblasts, Acta Biomater., 6(2010), No. 8, p. 3339.
    [2]
    R.D.K. Misra, W.W. Thein-Han, S.A. Mali, M.C. Somani, and L.P. Karjalainen, Cellular activity of bioactive nanograined/ultrafine-grained materials, Acta Biomater., 6(2010), No. 7, p. 2826.
    [3]
    S. Mali, R.D.K. Misra, M.C. Somani, and L.P. Karjalainen, Biomimetic nanostructured coatings on nano-grained/ultrafine-grained substrate:microstructure, surface adhesion strength, and biosolubility, Mater. Sci. Eng. C, 29(2009), No. 8, p. 2417.
    [4]
    P.K.C. Venkatsurya, W.W. Thein-Han, R.D.K. Misra, M.C. Somani, and L.P. Karjalainen, Advancing nanograined/ultrafine-grained structures for metal implant technology:interplay between grooving of nano/ultrafine grains and cellular response, Mater. Sci. Eng. C, 30(2010), No. 7, p. 1050.
    [5]
    R.D.K. Misra, B.R. Kumar, M. Somani, and P. Karjalainen, Deformation processes during tensile straining of ultrafine/nanograined structures formed by reversion in metastable austenitic steels, Scripta Mater., 59(2008), No. 1, p. 79.
    [6]
    B. Hwang and C.G. Lee, Influence of thermomechanical processing and heat treatments on tensile and Charpy impact properties of B and Cu bearing high-strength low-alloy steels, Mater. Sci. Eng. A, 527(2010), No. 16-17, p. 4341.
    [7]
    X.W. Kong, L.Y. Lan, Z.Y. Hu, B. Li, and T.Z. Sui, Optimization of mechanical properties of high strength bainitic steel using thermo-mechanical control and accelerated cooling process, J. Mater. Process. Technol., 217(2015), p. 202.
    [8]
    H.X. Yin, A.M. Zhao, Z.Z. Zhao, X. Li, S.J. Li, H.J. Hu, and W.G. Xia, Influence of original microstructure on the transformation behavior and mechanical properties of ultra-high-strength TRIP-aided steel, Int. J. Miner. Metall. Mater., 22(2015), No. 3, p. 262.
    [9]
    T. Sakai, A. Belyakov, R. Kaibyshev, H. Miura, and J.J. Jonas, Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions, Prog. Mater Sci., 60(2014), p. 130.
    [10]
    I.A. Yakubtsov, P. Poruks, and J.D. Boyd, Microstructure and mechanical properties of bainitic low carbon high strength plate steels, Mater. Sci. Eng. A, 480(2008), No. 1-2, p. 109.
    [11]
    X.X. Xu, Y. Yu, W.L. Cui, B.Z. Bai, and J.L. Gu, Ultra-high cycle fatigue behavior of high strength steel with carbide-free bainite/martensite complex microstructure, Int. J. Miner. Metall. Mater., 16(2009), No. 3, p. 285.
    [12]
    Y.Q. Weng, achievements of new generation steels program in china, Mater. Rev., 18(2004), p. 68.
    [13]
    M.M. Tong, J. Ni, Y.T. Zhang, D.Z. Li, and Y.Y. Li, Temporal oscillatory behavior in deformation induced ferrite transformation in an Fe-C binary system, Scripta Mater., 50(2004), No. 6, p. 909.
    [14]
    C. Garcia-Mateo, F.G. Caballero, and H.K.D.H. Bhadeshia, Development of hard bainite, ISIJ Int., 43(2003), No. 8, p. 1238.
    [15]
    F. Forouzan, A. Najafizadeh, A. Kermanpur, A. Hedayati, and R. Surkialiabad, Production of nano/submicron grained AISI 304L stainless steel through the martensite reversion process, Mater. Sci. Eng. A, 527(2010), No. 27, p. 7334.
    [16]
    R. Ueji, N. Tsuji, Y. Minamino, and Y. Koizumi, Ultragrain refinement of plain low carbon steel by cold-rolling and annealing of martensite, Acta Mater., 50(2002), No. 16, p. 4177.
    [17]
    W. Jiang, D. Ye, J. Li, J. Su, and K.Y. Zhao, Reverse transformation mechanism of martensite to austenite in 00Cr15Ni7Mo2WCu2 super martensitic stainless steel, Steel Res. Int., 85(2014), No. 7, p. 1150.
    [18]
    C. Ghosh, C. Aranas Jr., and J.J. Jonas, Dynamic transformation of deformed austenite at temperatures above the Ae3, Prog. Mater Sci., 82(2016), p. 151.
    [19]
    K. Tomimura, S. Takaki, and Y. Tokunaga, Reversion mechanism from deformation induced martensite to austenite in metastable austenitic stainless steels, ISIJ Int., 31(1991), No. 12, p. 1431.
    [20]
    A. Belyakov, K. Tsuzaki, H. Miura, and T. Sakai, Effect of initial microstructures on grain refinement in a stainless steel by large strain deformation, Acta Mater., 51(2003), No. 3, p. 847.
    [21]
    J. Han and Y.K. Lee, The effects of the heating rate on the reverse transformation mechanism and the phase stability of reverted austenite in medium Mn steels, Acta Mater., 67(2014), p. 354.
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Share Article

    Article Metrics

    Article Views(431) PDF Downloads(9) Cited by()
    Proportional views

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return