Chang-hong Chen, Ke-qin Feng, Yu Zhou,  and Hong-ling Zhou, Effect of sintering temperature on the microstructure and properties of foamed glass-ceramics prepared from high-titanium blast furnace slag and waste glass, Int. J. Miner. Metall. Mater., 24(2017), No. 8, pp. 931-936. https://doi.org/10.1007/s12613-017-1480-8
Cite this article as:
Chang-hong Chen, Ke-qin Feng, Yu Zhou,  and Hong-ling Zhou, Effect of sintering temperature on the microstructure and properties of foamed glass-ceramics prepared from high-titanium blast furnace slag and waste glass, Int. J. Miner. Metall. Mater., 24(2017), No. 8, pp. 931-936. https://doi.org/10.1007/s12613-017-1480-8
Research Article

Effect of sintering temperature on the microstructure and properties of foamed glass-ceramics prepared from high-titanium blast furnace slag and waste glass

+ Author Affiliations
  • Corresponding author:

    Ke-qin Feng    E-mail: kqfeng@scu.edu.cn

  • Received: 15 November 2016Revised: 12 March 2017Accepted: 14 March 2017
  • Foamed glass-ceramics were prepared via a single-step sintering method using high-titanium blast furnace slag and waste glass as the main raw materials The influence of sintering temperature (900-1060℃) on the microstructure and properties of foamed glass-ceramics was studied. The results show that the crystal shape changed from grainy to rod-shaped and finally turned to multiple shapes as the sintering temperature was increased from 900 to 1060℃. With increasing sintering temperature, the average pore size of the foamed glass-ceramics increased and subsequently decreased. By contrast, the compressive strength and the bulk density decreased and subsequently increased. An excessively high temperature, however, induced the coalescence of pores and decreased the compressive strength. The optimal properties, including the highest compressive strength (16.64 MPa) among the investigated samples and a relatively low bulk density (0.83 g/cm3), were attained in the case of the foamed glass-ceramics sintered at 1000℃.
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  • [1]
    J. König, R.R. Petersen, and Y.Z. Yue, Fabrication of highly insulating foam glass made from CRT panel glass, Ceram. Int., 41(2015), No. 8, p. 9793.
    [2]
    M. Reben, M. Kosmal, M. Ziąbka, P. Pichniarczyk, and I. Grelowska, The influence of TiO2 and ZrO2 on microstructure and crystallization behavior of CRT glass, J. Non-Cryst. Solids, 425(2015), No. 10, p. 118.
    [3]
    M.G. Zhu, R. Ji, Z.M. Li, H. Wang, L.L. Liu, and Z.T. Zhang, Preparation of glass ceramic foams for thermal insulation applications from coal fly ash and waste glass, Constr. Build. Mater., 112(2016), No. 1, p. 398.
    [4]
    E. Bernardo, G. Scarinci, P. Bertuzzi, P. Ercole, and L. Ramon, Recycling of waste glasses into partially crystallized glass foams, J. Porous Mater., 14(2010), No. 3, p. 359.
    [5]
    E. Bernardo and F. Albertini, Glass foams from dismantled cathode ray tubes, Ceram. Int., 32(2006), No. 6, p. 603.
    [6]
    J.G. Bai, X.H. Yang, S.C. Xu, W.J. Jing, and J.F. Yang, Preparation of foam glass from waste glass and fly ash, Mater. Lett., 136(2014), No. 14, p. 52.
    [7]
    Z. Liu, N.N. Shao, D.M. Wang, J.F. Qin, T.Y. Huang, W. Song, M.X. Lin, J.S. Yuan, and Z. Wang, Fabrication and properties of foam geopolymer using circulating fluidized bed combustion fly ash, Int. J. Miner. Metall. Mater., 21(2014), No. 1, p. 89.
    [8]
    Z. Li, Z.W. Luo, X.Y. Li, T.Y. Liu, L.M. Guan, T. Wu, and A.X. Lu, Preparation and characterization of glass-ceramic foams with waste quartz sand and coal gangue in different proportions, J. Porous Mater., 23(2016), No. 1, p. 231.
    [9]
    H. Sazegaran, A. Kiani-Rashid, and J.V. Khaki, Effects of sphere size on the microstructure and mechanical properties of ductile iron-steel hollow sphere syntactic foams, Int. J. Miner. Metall. Mater., 23(2016), No. 6, p. 676.
    [10]
    B. Chen, K.Q Wang, X.J. Chen, and A.X. Lu, Study of foam glass with high content of fly ash using calcium carbonate as foaming agent, Mater. Lett., 79(2012), No. 8, p. 263.
    [11]
    E. Ercenk, The effect of clay on foaming and mechanical properties of glass foam insulating material, J. Therm. Anal. Calorim., 127(2017), No. 1, p. 137.
    [12]
    H. Shi, K.Q. Feng, H.B. Wang, C.H. Chen, and H.L. Zhou, Influence of aluminium nitride as a foaming agent on the preparation of foam glass-ceramics from high-titanium blast furnace slag, Int. J. Miner. Metall. Mater., 23(2016), No. 5, p. 595.
    [13]
    R. Lebullenger, S. Chenu, J. Rocherullé, O. Merdrignac-Conanec, F. Cheviré, F. Tessier, A. Bouzaza, and S. Brosillon, Glass foams for environmental applications, J. Non-Cryst. Solids, 365(2010), No. 44-49, p. 2562.
    [14]
    P.K. Padhi and A. Satapathy, Analysis of sliding wear characteristics of BFS filled composites using an experimental design approach integrated with ANN, Tribol. Trans., 56(2013), No. 5, p. 789.
    [15]
    N. Sasmal, M. Garai, and B. Karmakar, Preparation and characterization of novel foamed porous glass-ceramics, Mater. Charact., 103(2015), No. 3, p. 90.
    [16]
    Y. Zhao, D.F. Chen, Y.Y. Bi, and M.J. Long, Preparation of low cost glass-ceramics from molten blast furnace slag, Ceram. Int., 38(2012), No. 3, p. 2495.
    [17]
    S. Hasheminia, A. Nemati, B.E. Yekta, and P. Alizadeh, Preparation and characterisation of diopside-based glass-ceramic foams, Ceram. Int., 38(2012), No. 3, p. 2005.
    [18]
    A.R.J. Barbosa, A.A.S. Lopes, S.I.H. Sequeira, J.P. Oliveira, A. Davarpanah, F. Mohseni, V.S. Amaral, and R.C.C. Monteiro, Effect of processing conditions on the properties of recycled cathode ray tube glass foams, J. Porous Mater., 23(2016), No. 6, p. 1663.
    [19]
    A. Goel, D.U. Tulyaganov, S. Agathopoulos, M.J. Ribeiro, and J.M.F. Ferreira, Crystallization behaviour, structure and properties of sintered glasses in the diopside-Ca-Tschermak system, J. Eur. Ceram. Soc., 27(2007), No. 10, p. 3231.
    [20]
    L. Liu, M.L. Hu, C.G. Bai, X.W. Lü, Y.Z. Xu, and Q.Y. Deng, Effect of cooling rate on the crystallization behavior of perovskite in high titanium-bearing blast furnace slag, Int. J. Miner. Metall. Mater., 21(2014), No. 11, p. 1052.
    [21]
    Z.S. Ren, X.J. Hu, X.M. Hou, X.X. Xue, and K.C. Chou, Dissolution and diffusion of TiO2 in the CaO-Al2O3-SiO2 slag, Int. J. Miner. Metall. Mater., 21(2014), No. 4, p. 345.
    [22]
    B.S. Tang, J. Lin, S. Qian, J.D Wang, and S. Zhang, Preparation of glass-ceramic foams from the municipal solid waste slag produced by plasma gasification process, Mater. Lett., 128(2014), No. 8, p. 68.
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