Understanding micro-diffusion bonding from the fabrication of B<sub>4</sub>C/Ni composites

Miao Wang; Wen-xian Wang; Hong-sheng Chen; Yu-li Li

doi:10.1007/s12613-018-1580-0

Volume 25 Issue 3

Mar. 2018

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Article Navigation > International Journal of Minerals, Metallurgy and Materials > 2018 > 25(3): 365-374

Miao Wang, Wen-xian Wang, Hong-sheng Chen, and Yu-li Li, Understanding micro-diffusion bonding from the fabrication of B₄C/Ni composites, Int. J. Miner. Metall. Mater., 25(2018), No. 3, pp. 365-374. https://doi.org/10.1007/s12613-018-1580-0

Cite this article as:

Miao Wang, Wen-xian Wang, Hong-sheng Chen, and Yu-li Li, Understanding micro-diffusion bonding from the fabrication of B4C/Ni composites, Int. J. Miner. Metall. Mater., 25(2018), No. 3, pp. 365-374. https://doi.org/10.1007/s12613-018-1580-0

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Research Article

Understanding micro-diffusion bonding from the fabrication of B₄C/Ni composites

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Corresponding author:
Wen-xian Wang E-mail: wangwenxian@tyut.edu.cn
Received: 28 April 2017; Revised: 25 November 2017; Accepted: 8 December 2017

Abstract

Abstract

A Ni-B₄C macroscopic diffusion welding couple and a Ni-15wt%B₄C composite fabricated by spark plasma sintering (SPS) were used to understand the micro-scale diffusion bonding between metals and ceramics. In the Ni-B₄C macroscopic diffusion welding couple a perfect diffusion welding joint was achieved. In the Ni-15wt%B₄C sample, microstructure analyses demonstrated that loose structures occurred around the B₄C particles. Energy dispersive X-ray spectroscopy analyses revealed that during the SPS process, the process of diffusion bonding between Ni and B₄C particles can be divided into three stages. By employing a nano-indentation test, the room-temperature fracture toughness of the Ni matrix was found to be higher than that of the interface. The micro-diffusion bonding between Ni and B₄C particles is quite different from the Ni-B₄C reaction couple.
- B₄C/Ni composites;
- spark plasma sintering;
- micro-diffusion welding;
- microstructure;
- nano-mechanical property

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