摘要:
Oxide eutectic ceramic
in situ composites have attracted significant interest in the application of high-temperature structural materials because of their excellent high-temperature strength, oxidation and creep resistance, as well as outstanding microstructural stability. The directionally solidified ternary Al
2O
3/YAG/ZrO
2 hypereutectic
in situ composite was successfully prepared by a laser zone remelting method, aiming to investigate the growth characteristic under ultra-high temperature gradient. The microstructures and phase composition of the as-solidified hypereutectic were characterized by using scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD). The results show that the composite presents a typical hypereutectic lamellar microstructure consisting of fine Al
2O
3 and YAG phases, and the enriched ZrO
2 phases with smaller sizes are randomly distributed at the Al
2O
3/YAG interface and in Al
2O
3 phases. Laser power and scanning rate strongly affect the sample quality and microstructure characteristic. Additionally, coarse colony microstructures were also observed, and their formation and the effect of temperature gradient on the microstructure were discussed.