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Volume 19 Issue 5
May  2012
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E. Ghomash Pasand, A. Nemati, M. Solati-Hashjin, K. Arzani, and A. Farzadi, Microwave assisted synthesis & properties of nano HA-TCP biphasic calcium phosphate, Int. J. Miner. Metall. Mater., 19(2012), No. 5, pp. 441-445. https://doi.org/10.1007/s12613-012-0576-4
Cite this article as:
E. Ghomash Pasand, A. Nemati, M. Solati-Hashjin, K. Arzani, and A. Farzadi, Microwave assisted synthesis & properties of nano HA-TCP biphasic calcium phosphate, Int. J. Miner. Metall. Mater., 19(2012), No. 5, pp. 441-445. https://doi.org/10.1007/s12613-012-0576-4
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Microwave assisted synthesis & properties of nano HA-TCP biphasic calcium phosphate

  • 通讯作者:

    A. Nemati    E-mail: nemati@sharif.edu

  • Biphasic calcium phosphate (BCP) nanopowders were synthesized by using microwave and non-microwave irradiation assisted processes. The synthesized powders were pressed under a pressure of 90 MPa, and then were sintered at 1000-1200℃ for 1 h. The mechanical properties of the samples were investigated. The formed phases and microstructures were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results showed that the synthesis time was shorter, along with a more homogeneous microstructure, when the microwave irradiation assisted method was applied. The compression strength and the Young's modulus of the samples synthesized with microwave irradiation were about 60 MPa and 3 GPa, but those of the samples synthesized without microwave irradiation were about 30 MPa and 2 GPa, respectively. XRD patterns of the microwave irradiation assisted and non-microwave irradiation assisted nanopowders showed the coexistence of hydroxyapatite (HA) and tricalcium phosphate (TCP) phases in the system.
  • Microwave assisted synthesis & properties of nano HA-TCP biphasic calcium phosphate

    + Author Affiliations
    • Biphasic calcium phosphate (BCP) nanopowders were synthesized by using microwave and non-microwave irradiation assisted processes. The synthesized powders were pressed under a pressure of 90 MPa, and then were sintered at 1000-1200℃ for 1 h. The mechanical properties of the samples were investigated. The formed phases and microstructures were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results showed that the synthesis time was shorter, along with a more homogeneous microstructure, when the microwave irradiation assisted method was applied. The compression strength and the Young's modulus of the samples synthesized with microwave irradiation were about 60 MPa and 3 GPa, but those of the samples synthesized without microwave irradiation were about 30 MPa and 2 GPa, respectively. XRD patterns of the microwave irradiation assisted and non-microwave irradiation assisted nanopowders showed the coexistence of hydroxyapatite (HA) and tricalcium phosphate (TCP) phases in the system.
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