Synthesis of WC powder through microwave heating of WO<sub>3</sub>-C mixture

Amir Karimzadeh Behnami; Arman Hoseinpur; Masoud Sakaki; Mohammad Sh. Bafghi; Kazumichi Yanagisawa

doi:10.1007/s12613-017-1396-3

Volume 24 Issue 2

Feb. 2017

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文章导航 > 矿物冶金与材料学报（英文） > 2017 > 24(2): 202-207

Amir Karimzadeh Behnami, Arman Hoseinpur, Masoud Sakaki, Mohammad Sh. Bafghi, and Kazumichi Yanagisawa, Synthesis of WC powder through microwave heating of WO₃-C mixture, Int. J. Miner. Metall. Mater., 24(2017), No. 2, pp. 202-207. https://doi.org/10.1007/s12613-017-1396-3

Cite this article as:

Amir Karimzadeh Behnami, Arman Hoseinpur, Masoud Sakaki, Mohammad Sh. Bafghi, and Kazumichi Yanagisawa, Synthesis of WC powder through microwave heating of WO3-C mixture, Int. J. Miner. Metall. Mater., 24(2017), No. 2, pp. 202-207. https://doi.org/10.1007/s12613-017-1396-3

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研究论文

Synthesis of WC powder through microwave heating of WO₃-C mixture

School of Metallurgy and Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran 16846-13114, Iran
Department of Materials Engineering, Faculty of Engineering, Malayer University, Malayer 65719-95863, Iran
Research Laboratory of Hydrothermal Chemistry, Faculty of Science, Kochi University, Kochi 780-8073, Japan

通讯作者:
Masoud Sakaki E-mail: masoudsakaki79@gmail.com

中文摘要

A simple, easy, and low-cost process for the fabrication of tungsten carbide (WC) powder through microwave heating of WO₃-C mixtures was developed. Thermodynamic calculations and experimental investigations were carried out for WO₃-C and W-C systems, and a formation mechanism was proposed. In the results, for the synthesis of WC, the use of over stoichiometric amount of C together with a specially assembled experimental setup (which effectively retains heat in the system) is necessary. The WC powder is successfully obtained by heating WO₃:5C mixture for 900s in a domestic microwave oven.

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Research Article

Synthesis of WC powder through microwave heating of WO₃-C mixture

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Abstract

Abstract

A simple, easy, and low-cost process for the fabrication of tungsten carbide (WC) powder through microwave heating of WO₃-C mixtures was developed. Thermodynamic calculations and experimental investigations were carried out for WO₃-C and W-C systems, and a formation mechanism was proposed. In the results, for the synthesis of WC, the use of over stoichiometric amount of C together with a specially assembled experimental setup (which effectively retains heat in the system) is necessary. The WC powder is successfully obtained by heating WO₃:5C mixture for 900s in a domestic microwave oven.
- tungsten carbide;
- microwave heating;
- carbothermic reduction;
- thermodynamic analysis

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Synthesis of WC powder through microwave heating of WO₃-C mixture

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Synthesis of WC powder through microwave heating of WO₃-C mixture

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