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Hao Liu, Nan Wei, Zhou-fu Wang, Xi-tang Wang, and Yan Ma, Fabrication and properties of aluminum silicate fibrous materials with in situ synthesized K2Ti6O13 whiskers, Int. J. Miner. Metall. Mater., 24(2017), No. 11, pp.1335-1340. https://dx.doi.org/10.1007/s12613-017-1525-z
Hao Liu, Nan Wei, Zhou-fu Wang, Xi-tang Wang, and Yan Ma, Fabrication and properties of aluminum silicate fibrous materials with in situ synthesized K2Ti6O13 whiskers, Int. J. Miner. Metall. Mater., 24(2017), No. 11, pp.1335-1340. https://dx.doi.org/10.1007/s12613-017-1525-z
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Fabrication and properties of aluminum silicate fibrous materials with in situ synthesized K2Ti6O13 whiskers

摘要: To improve their mechanical and thermal insulation properties, aluminum silicate fibrous materials with in situ synthesized K2Ti6O13 whiskers were prepared by firing a mixture of short aluminum silicate fibers and gel powders obtained from a sol-gel process. During the preparation process, the fiber surface was coated with K2Ti6O13 whiskers after the fibers were subjected to a heat treatment carried out at various temperatures. The effects of process parameters on the microstructure, compressive strength, and thermal conductivity were analyzed systematically. The results show that higher treatment temperatures and longer treatment durations promoted the development of K2Ti6O13 whiskers on the surface of aluminum silicate fibers; in addition, the intersection structure between whiskers modulated the morphology and volume of the multi-aperture structure among fibers, substantially increasing the fibers' compressive strength and reducing their heat conduction and convective heat transfer at high temperatures.

 

Fabrication and properties of aluminum silicate fibrous materials with in situ synthesized K2Ti6O13 whiskers

Abstract: To improve their mechanical and thermal insulation properties, aluminum silicate fibrous materials with in situ synthesized K2Ti6O13 whiskers were prepared by firing a mixture of short aluminum silicate fibers and gel powders obtained from a sol-gel process. During the preparation process, the fiber surface was coated with K2Ti6O13 whiskers after the fibers were subjected to a heat treatment carried out at various temperatures. The effects of process parameters on the microstructure, compressive strength, and thermal conductivity were analyzed systematically. The results show that higher treatment temperatures and longer treatment durations promoted the development of K2Ti6O13 whiskers on the surface of aluminum silicate fibers; in addition, the intersection structure between whiskers modulated the morphology and volume of the multi-aperture structure among fibers, substantially increasing the fibers' compressive strength and reducing their heat conduction and convective heat transfer at high temperatures.

 

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