Effects of aluminum and titanium on the microstructure of ODS steels fabricated by hot pressing

Qian Zhao, Li-ming Yu, Yong-chang Liu, Yuan Huang, Zong-qing Ma, Hui-jun Li

分享

计量
  • 文章访问数:  580
  • HTML全文浏览量:  104
  • PDF下载量:  20
  • 被引次数: 34

目录

Cite this article as:

Qian Zhao, Li-ming Yu, Yong-chang Liu, Yuan Huang, Zong-qing Ma, and Hui-jun Li, Effects of aluminum and titanium on the microstructure of ODS steels fabricated by hot pressing, Int. J. Miner. Metall. Mater., 25(2018), No. 10, pp.1156-1165. https://dx.doi.org/10.1007/s12613-018-1667-7
Qian Zhao, Li-ming Yu, Yong-chang Liu, Yuan Huang, Zong-qing Ma, and Hui-jun Li, Effects of aluminum and titanium on the microstructure of ODS steels fabricated by hot pressing, Int. J. Miner. Metall. Mater., 25(2018), No. 10, pp.1156-1165. https://dx.doi.org/10.1007/s12613-018-1667-7
引用本文 PDF XML SpringerLink
研究论文

Effects of aluminum and titanium on the microstructure of ODS steels fabricated by hot pressing

基金项目: 

This work was financially supported by the National Natural Science Foundation of China (Nos. 51474156 and U1660201) and the National Magnetic Confinement Fusion Energy Research Project (No. 2015GB119000).

    通信作者:

    Li-ming Yu E-mail: lmyu@tju.edu.cn

    Yong-chang Liu E-mail: ycliu@tju.edu.cn

Three oxide-dispersion-strengthened (ODS) steels with compositions of Fe-14Cr-2W-0.2V-0.07Ta-0.3Y2O3 (wt%, so as the follows) (14Y), Fe-14Cr-2W-0.2V-0.07Ta-1Al-0.3Y2O3 (14YAl), and Fe-14Cr-2W-0.2V-0.07Ta-0.3Ti-0.3 Y2O3 (14YTi) were fabricated by hot pressing. Transmission electron microscopy (TEM) was used to characterize the microstructures and nanoparticles of these ODS steels. According to the TEM results, 14Y, 14YAl, and 14YTi ODS steels present similar bimodal structures containing both large and small grains. The addition of Al or Ti has no obvious effect on the microstructure of the steels. The spatial and size distribution of the nanoparticles was also analyzed. The results indicate that the average size of nanoparticles in the 14YTi ODS steel is smaller than that in the 14YAl ODS steel. Nanoparticles such as Y2O3, Y3Al5O12 and YAlO3, and Y2Ti2O7 were identified in the 14Y, 14YAl, and 14YTi ODS steels, respectively.

 

Research Article

Effects of aluminum and titanium on the microstructure of ODS steels fabricated by hot pressing

Author Affilications
  • Funds: 

    This work was financially supported by the National Natural Science Foundation of China (Nos. 51474156 and U1660201) and the National Magnetic Confinement Fusion Energy Research Project (No. 2015GB119000).

  • Received: 29 January 2018; Revised: 04 March 2018; Accepted: 05 March 2018;
Three oxide-dispersion-strengthened (ODS) steels with compositions of Fe-14Cr-2W-0.2V-0.07Ta-0.3Y2O3 (wt%, so as the follows) (14Y), Fe-14Cr-2W-0.2V-0.07Ta-1Al-0.3Y2O3 (14YAl), and Fe-14Cr-2W-0.2V-0.07Ta-0.3Ti-0.3 Y2O3 (14YTi) were fabricated by hot pressing. Transmission electron microscopy (TEM) was used to characterize the microstructures and nanoparticles of these ODS steels. According to the TEM results, 14Y, 14YAl, and 14YTi ODS steels present similar bimodal structures containing both large and small grains. The addition of Al or Ti has no obvious effect on the microstructure of the steels. The spatial and size distribution of the nanoparticles was also analyzed. The results indicate that the average size of nanoparticles in the 14YTi ODS steel is smaller than that in the 14YAl ODS steel. Nanoparticles such as Y2O3, Y3Al5O12 and YAlO3, and Y2Ti2O7 were identified in the 14Y, 14YAl, and 14YTi ODS steels, respectively.

 

  • A. Kimura, Current status of reduced-activation ferritic/martensitic steels R&D for fusion energy, Mater. Trans., 46(2005), No. 3, p. 394.

    J.P. Wharry, M.J. Swenson, and K.H. Yano, A review of the irradiation evolution of dispersed oxide nanoparticles in the b.c.c. Fe-Cr system:Current understanding and future directions, J. Nucl. Mater., 486(2017), p. 11.

    L. Raman, K. Gothandapani, and B.S. Murty, Austenitic oxide dispersion strengthened steels:A review, Defence Sci. J., 66(2016), No. 4, p. 316.

    K. Verhiest, A. Almazouzi, N. De Wispelaere, R. Petrov, and S. Claessens, Development of oxides dispersion strengthened steels for high temperature nuclear reactor applications, J. Nucl. Mater., 385(2009), No. 2, p. 308.

    G.R. Odette, M.J. Alinger, and B.D. Wirth, Recent developments in irradiation-resistant steels, Annu. Rev. Mater. Res., 38(2008), p. 471.

    G.R. Odette, Recent progress in developing and qualifying nanostructured ferritic alloys for advanced fission and fusion applications, JOM, 66(2014), No. 12, p. 2427.

    T.K. Kim, S. Noh, S.H. Kang, J.P. Jin, H.J. Jin, K.L. Min, J. Jang, and C.K. Rhee, Current status and future prospective of advanced radiation resistant oxide dispersion strengthened steel (ARROS) development for nuclear reactor system applications, Nucl. Eng. Technol., 48(2016), No. 2, p. 572.

    Q. Zhao, L.M. Yu, Y.C. Liu, Y. Huang, Q.Y. Guo, H.J. Li, and J.F. Wu, Evolution of Al-containing phases in ODS steel by hot pressing and annealing, Powder Technol., 311(2017), p. 449.

    Q. Zhao, L.M. Yu, Y.C. Liu, Y. Huang, Z.Q. Ma, H.J. Li, and J.F. Wu, Microstructure and tensile properties of a 14Cr ODS ferritic steel, Mater. Sci. Eng. A, 680(2017), p. 347.

    W. Li, T. Hao, R. Gao, X.P. Wang, T. Zhang, Q.F. Fang, and C.S. Liu, The effect of Zr, Ti addition on the particle size and microstructure evolution of yttria nanoparticle in ODS steel, Powder Technol., 319(2017), p. 172.

    P. Olier, M. Couvrat, C. Cayron, N. Lochet, and L. Chaffron, Incidence of mechanical alloying contamination on oxides and carbides formation in ODS ferritic steels, J. Nucl. Mater., 442(2013), No. 1-3, Suppl. 1, p. S106.

    M. Magini, A. Iasonna, and F. Padella, Ball milling:An experimental support to the energy transfer evaluated by the collision model, Scripta Mater., 34(1996), No. 1, p. 172.

    M. Nagini, R. Vijay, M. Ramakrishna, A.V. Reddy, and G. Sundararajan, Influence of the duration of high energy ball milling on the microstructure and mechanical properties of a 9Cr oxide dispersion strengthened ferritic-martensitic steel, Mater. Sci. Eng. A, 620(2017), p. 490.

    C. Suryanarayana, Mechanical alloying and milling, Prog. Mater. Sci., 46(2001), No. 1-2, p. 1.

    I. Hilger, X. Boulnat, J. Hoffmann, C. Testani, F. Bergner, Y. De Carlan, F. Ferraro, and A. Ulbricht, Fabrication and characterization of oxide dispersion strengthened (ODS) 14Cr steels consolidated by means of hot isostatic pressing, hot extrusion and spark plasma sintering, J. Nucl. Mater., 472(2017), p. 206.

    X.S. Zhou, C.X. Liu, L.M. Yu, Y.C. Liu, and H.J. Li, Phase transformation behavior and microstructural control of high-Cr martensitic/ferritic heat-resistant steels for power and nuclear plants:a review, J. Mater. Sci. Technol., 31(2015), No. 3, p. 235.

    B. Mouawad, X. Boulnat, D. Fabrègue, M. Perez, and Y. de Carlan, Tailoring the microstructure and the mechanical properties of ultrafine grained high strength ferritic steels by powder metallurgy, J. Nucl. Mater., 465(2015), p. 54.

    D.T. Hoelzer, K.A. Unocic, M.A. Sokolov, and T.S. Byun, Influence of processing on the microstructure and mechanical properties of 14YWT, J. Nucl. Mater., 471(2016), p. 251.

    B. van der Schaaf, F. Tavassoli, C. Fazio, E. Rigal, E. Diegele, R. Lindau, and G. LeMarois, The development of EUROFER reduced activation steel, Fusion Eng. Des., 69(2003), No. 1-4, p. 197.

    Z. Oksiuta, M. Lewandowska, P. Unifantowicz, N. Baluc, and K.J. Kurzydlowski, Influence of Y2O3 and Fe2Y additions on the formation of nano-scale oxide particles and the mechanical properties of an ODS RAF steel, Fusion Eng. Des., 86(2011), No. 9-11, p. 2417.

    A. Kimura, R. Kasada, N. Iwata, H. Kishimoto, C.H. Zhang, J. Isselin, P. Dou, J.H. Lee, N. Muthukumar, T. Okuda, M. Inoue, S. Ukai, S. Ohnuki, T. Fujisawa, and T.F. Abe, Development of Al added high-Cr ODS steels for fuel cladding of next generation nuclear systems, J. Nucl. Mater., 417(2011), No. 1-3, p. 176.

    R. Gao, L.L. Xia, T. Zhang, X.P. Wang, Q.F. Fang, and C.S. Liu, Oxidation resistance in LBE and air and tensile properties of ODS ferritic steels containing Al/Zr elements, J. Nucl. Mater., 455(2014), No. 1-3, p. 407.

    C. Capdevila, G. Pimentel, M.M. Aranda, R. Rementeria, K. Dawson, E. Urones-Garrote, G.J. Tatlock, and M.K. Miller, Role of Y-Al oxides during extended recovery process of a ferritic ODS alloy, JOM, 67(2015), No. 10, p. 2208.

    P. He, M. Klimenkov, R. Lindau, and A. Möslang, Characterization of precipitates in nano structured 14% Cr ODS alloys for fusion application, J. Nucl. Mater., 428(2012), No. 1-3, p. 131.

    J. Chao, R. Rementeria, M. Aranda, C. Capdevila, and J. Gonzalezcarrasco, Comparison of ductile-to-brittle transition behavior in two similar ferritic oxide dispersion strengthened alloys, Materials, 9(2016), No. 8, p. 637.

    J.M. Torralba, L. Fuentes-Pacheco, N. García-Rodríguez, and M. Campos, Development of high performance powder metallurgy steels by high-energy milling, Adv. Powder Technol., 24(2013), No. 5, p. 813.

    T. Liu, L.B. Wang, C.X. Wang, and H.L. Shen, Effect of Al content on the oxidation behavior of Y2Ti2O7-dispersed Fe-14Cr ferritic alloys, Corros. Sci., 104(2016), p. 17.

    J.S. Lee, C.H. Jang, I.S. Kim, and A. Kimura, Embrittlement and hardening during thermal aging of high Cr oxide dispersion strengthened alloys, J. Nucl. Mater., 367-370(2007), p. 229.

    X.Y. Yuan, Z. Yang, X. Li, and L.Q. Chen, Effect of Cr on mechanical properties and corrosion behaviors of Fe-Mn-C-Al-Cr-N TWIP steels, J. Mater. Sci. Technol., 33(2017), No. 12, p. 1555.

    S.F. Li, Z.J. Zhou, P.H. Wang, H.Y. Sun, M. Wang, and G.M. Zhang, Long-term thermal-aging stability of a 16Cr-oxide dispersion strengthened ferritic steel at 973 K, Mater. Des., 90(2016), p. 318.

    R. Chinnappan, Thermodynamic stability of oxide phases of Fe-Cr based ODS steels via quantum mechanical calculations, Calphad, 45(2014), p. 188.

    X. Zhao, L.C. Guo, L. Zhang, T.T. Jia, C.G. Chen, J.J. Hao, H.P. Shao, Z.M. Guo, J. Luo, and J.B. Sun, Influence of nano-Al2O3-reinforced oxide-dispersion-strengthened Cu on the mechanical and tribological properties of Cu-based composites, Int. J. Miner. Metall. Mater., 23(2016), No. 12, p. 1444.

Relative Articles

C. D. Gómez-Esparza, A. Duarte-Moller, C. López-Díaz de León, R. Martínez-Sánchez, J. F. Hernández-Paz, C. A. Rodríguez-González. Influence of ZnO nanoparticles on the microstructure of a CoCrFeMoNi matrix via powder metallurgy [J]. 矿物冶金与材料学报(英文版). DOI: 10.1007/s12613-019-1863-0

View details

Chun-fu Kuang, Zhi-wang Zheng, Min-li Wang, Quan Xu, Shen-gen Zhang. Effect of hot-dip galvanizing processes on the microstructure and mechanical properties of 600-MPa hot-dip galvanized dual-phase steel [J]. 矿物冶金与材料学报(英文版). DOI: 10.1007/s12613-017-1530-2

View details

Deepak Pathania, Rishu Katwal, Harpreet Kaur. Enhanced photocatalytic activity of electrochemically synthesized aluminum oxide nanoparticles [J]. 矿物冶金与材料学报(英文版). DOI: 10.1007/s12613-016-1245-9

View details

Lin-lin Yuan, Jing-tao Han, Jing Liu, Dong-bin Wei, Mehari Zelalem Abathun. Titanium effect on the microstructure and properties of laminated high boron steel plates [J]. 矿物冶金与材料学报(英文版). DOI: 10.1007/s12613-015-1098-7

View details

Zahra Hejri, Ali Akbar Seifkordi, Ali Ahmadpour, Seyed Mojtaba Zebarjad, Abdolmajid Maskooki. Biodegradable starch/poly (vinyl alcohol) film reinforced with titanium dioxide nanoparticles [J]. 矿物冶金与材料学报(英文版). DOI: 10.1007/s12613-013-0827-z

View details

Ali Rasooli, Mehdi Divandari, Hamid Reza Shahverdi, Mohammad Ali Boutorabi. Kinetics and mechanism of titanium hydride powder and aluminum melt reaction [J]. 矿物冶金与材料学报(英文版). DOI: 10.1007/s12613-012-0533-2

View details

Lianfeng Guo, Wenguang Zhang, Chengtao Wang. Preparation and crystallization control of nanoparticle hydroxyapatlte [J]. 矿物冶金与材料学报(英文版).

View details

Benfu Hu, Shunmi Peng, H Takahashi. Irradiation Damage of Oxide Dispersion Strengthened Ferritic Steel after Recrystallization [J]. 矿物冶金与材料学报(英文版).

View details

Citing articles(34)

Chunjie She, Guojun Chen, Xingwei Pei, et al. In Situ Observation of the Desulfurization of the Molten Steel by CaO–Al2O3 Desulfurizers. Metallurgical and Materials Transactions B, 2025. 必应学术
N. Preisser, Y. Wang, J. Cejka, et al. Application of high-temperature confocal scanning laser microscopy to investigate non-metallic inclusions in steel: a review. Journal of Iron and Steel Research International, 2025, 32(2): 334. 必应学术
Weijian Wang, Yuan Gao, Ying Ren, et al. Observation of Initial Interfacial Reaction between High Aluminum Molten Steel and CaO–Al2O3 Inclusion at 1873 K Using Laser Confocal Scanning Microscopy and Micro‐Computerized Tomography. steel research international, 2025, 96(1) 必应学术
More >

/

返回文章
返回