Crystalline texture evolution, control of the tribocorrosion behavior, and significant enhancement of the abrasion properties of a Ni-P nanocomposite coating enhanced by zirconia nanoparticles

Masoud Sabzi; Saeid Mersagh Dezfuli; Zohre Balak

doi:10.1007/s12613-019-1805-x

Volume 26 Issue 8

Aug. 2019

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文章导航 > 矿物冶金与材料学报（英文） > 2019 > 26(8): 1020-1030

Masoud Sabzi, Saeid Mersagh Dezfuli, and Zohre Balak, Crystalline texture evolution, control of the tribocorrosion behavior, and significant enhancement of the abrasion properties of a Ni-P nanocomposite coating enhanced by zirconia nanoparticles, Int. J. Miner. Metall. Mater., 26(2019), No. 8, pp. 1020-1030. https://doi.org/10.1007/s12613-019-1805-x

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Masoud Sabzi, Saeid Mersagh Dezfuli, and Zohre Balak, Crystalline texture evolution, control of the tribocorrosion behavior, and significant enhancement of the abrasion properties of a Ni-P nanocomposite coating enhanced by zirconia nanoparticles, Int. J. Miner. Metall. Mater., 26(2019), No. 8, pp. 1020-1030. https://doi.org/10.1007/s12613-019-1805-x

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Crystalline texture evolution, control of the tribocorrosion behavior, and significant enhancement of the abrasion properties of a Ni-P nanocomposite coating enhanced by zirconia nanoparticles

Young Researchers and Elite Club, Dezful Branch, Islamic Azad University, Dezful 6461645165, Iran
Department of Materials Science and Engineering, Science and Research Branch, Islamic Azad University, Tehran 1477893855, Iran
Department of Materials Science, Islamic Azad University, Ahwaz 6224927333, Iran

通讯作者:
Saeid Mersagh Dezfuli E-mail: saeed.m.dezfooli@gmail.com

中文摘要

This paper describes an investigation of the effect of ZrO₂ nanoparticles on the abrasive properties, crystalline texture developments, and tribocorrosion behavior of Ni-P nanostructured coatings. In the investigation, Ni-P and Ni-P-ZrO₂ nanostructured coatings are deposited on St52 steel via the electroless method. Transmission electron microscopy (TEM), field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD), energy dispersive spectroscopy (EDS), cyclic-static polarization tests in 3.5wt% NaCl solution, the tribocorrosion test (by back-and-forth wear in electrochemical cell), and the microhardness test using the Vickers method were performed to characterize and analyze the deposited coatings. The results of this study showed that the addition of ZrO₂ nanoparticles to the Ni-P electroless bath produced the following:a sharp increase in wear and hardness resistance, the change of the wear mechanism from sheet to adhesive mode, the reduction of pitting corrosion resistance, significant reduction in the tribocorrosion protective properties, change in the preferred orientation of the crystalline texture coating from (111) to (200), increase in the sedimentation rate during the deposit process, and a sharp increase in the thickness of the Ni-P nanostructured coatings.

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Research Article

Crystalline texture evolution, control of the tribocorrosion behavior, and significant enhancement of the abrasion properties of a Ni-P nanocomposite coating enhanced by zirconia nanoparticles

+ Author Affiliations

Abstract

Abstract

This paper describes an investigation of the effect of ZrO₂ nanoparticles on the abrasive properties, crystalline texture developments, and tribocorrosion behavior of Ni-P nanostructured coatings. In the investigation, Ni-P and Ni-P-ZrO₂ nanostructured coatings are deposited on St52 steel via the electroless method. Transmission electron microscopy (TEM), field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD), energy dispersive spectroscopy (EDS), cyclic-static polarization tests in 3.5wt% NaCl solution, the tribocorrosion test (by back-and-forth wear in electrochemical cell), and the microhardness test using the Vickers method were performed to characterize and analyze the deposited coatings. The results of this study showed that the addition of ZrO₂ nanoparticles to the Ni-P electroless bath produced the following:a sharp increase in wear and hardness resistance, the change of the wear mechanism from sheet to adhesive mode, the reduction of pitting corrosion resistance, significant reduction in the tribocorrosion protective properties, change in the preferred orientation of the crystalline texture coating from (111) to (200), increase in the sedimentation rate during the deposit process, and a sharp increase in the thickness of the Ni-P nanostructured coatings.
- Ni-P nanocomposite coatings;
- ZrO₂ nanoparticles;
- crystalline texture;
- corrosion resistance;
- abrasive properties;
- tribocorrosion behavior

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References

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Crystalline texture evolution, control of the tribocorrosion behavior, and significant enhancement of the abrasion properties of a Ni-P nanocomposite coating enhanced by zirconia nanoparticles

中文摘要

Crystalline texture evolution, control of the tribocorrosion behavior, and significant enhancement of the abrasion properties of a Ni-P nanocomposite coating enhanced by zirconia nanoparticles

Abstract

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