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Zedong Wang, Kaibo Nie, Kunkun Deng, and Jungang Han, Effect of extrusion on the microstructure and mechanical properties of a low-alloyed Mg–2Zn–0.8Sr–0.2Ca matrix composite reinforced by TiC nano-particles, Int. J. Miner. Metall. Mater., 29(2022), No. 11, pp.1981-1990. https://dx.doi.org/10.1007/s12613-021-2353-8
Zedong Wang, Kaibo Nie, Kunkun Deng, and Jungang Han, Effect of extrusion on the microstructure and mechanical properties of a low-alloyed Mg–2Zn–0.8Sr–0.2Ca matrix composite reinforced by TiC nano-particles, Int. J. Miner. Metall. Mater., 29(2022), No. 11, pp.1981-1990. https://dx.doi.org/10.1007/s12613-021-2353-8
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挤压对TiC纳米颗粒增强低合金化Mg–2Zn–0.8Sr–0.2Ca基复合材料显微组织和力学性能的影响

摘要: 镁合金作为轻金属材料的代表,在电子、交通和航空航天等领域有着广阔的应用前景。然而镁合金仍存在强度低、延展性差和耐蚀性差等缺点,改善镁合金的强塑性已成为拓宽镁合金在工业应用的中的首要问题。本文利用超声辅助半固态搅拌法成功制备了TiC纳米颗粒增强低合金化Mg–2Zn–0.8Sr–0.2Ca基复合材料,并且对铸态复合材料进行热挤压变形,系统研究了挤压对其显微组织及力学性能的影响。结果表明,在较低的挤压温度或挤压速率下,复合材料动态再结晶的体积分数和再结晶晶粒尺寸有所降低。挤压条件为200°C, 0.1 mm/s时,复合材料中出现了晶粒尺寸约0.3 µm的细晶组织。挤压后的复合材料呈现强基面织构,当挤压温度从200℃增加到240℃时,基面织构强度随之增加。挤压条件为200°C,0.1 mm/s时复合材料的抗拉强度达480.2 MPa,屈服强度为462 MPa。对其强化机制进行理论计算表明相比与其他强化机制,细晶强化对强度的贡献最大。通过分析三种挤压后的纳米复合材料断裂行为,表明其断裂方式为韧脆混合型断裂。

 

Effect of extrusion on the microstructure and mechanical properties of a low-alloyed Mg–2Zn–0.8Sr–0.2Ca matrix composite reinforced by TiC nano-particles

Abstract: A low-alloyed Mg–2Zn–0.8Sr–0.2Ca matrix composite reinforced by TiC nano-particles was successfully prepared by semi-solid stirring under the assistance of ultrasonic, and then the as-cast composite was hot extruded. The results indicated that the volume fraction of dynamical recrystallization and the recrystallized grain size have a certain decline at lower extrusion temperature or rate. The finest grain size of ~0.30 µm is obtained in the sample extruded at 200°C and 0.1 mm/s. The as-extruded sample displays a strong basal texture intensity, and the basal texture intensity increases to 5.937 mud while the extrusion temperature increases from 200 to 240°C. The ultra-high mechanical properties (ultimate tensile strength of 480.2 MPa, yield strength of 462 MPa) are obtained after extrusion at 200°C with a rate of 0.1 mm/s. Among all strengthening mechanisms for the present composite, the grain refinement contributes the most to the increase in strength. A mixture of cleavage facets and dimples were observed in the fracture surfaces of three as-extruded nanocomposites, which explain a mix of brittle-ductile fracture way of the samples.

 

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