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Akanksha Dwivedi, K.E.R.V. Prasad, Debdipta Banik, Saikat Mandal, A. Durga Prasad, and Srinu Gangolu, Characterization of heat treatment-driven microstructural evolution, mechanical properties, and electrochemical behavior of direct powder forged Al–10Si–0.3Mg alloy, Int. J. Miner. Metall. Mater., (2026). https://doi.org/10.1007/s12613-025-3221-8
Akanksha Dwivedi, K.E.R.V. Prasad, Debdipta Banik, Saikat Mandal, A. Durga Prasad, and Srinu Gangolu, Characterization of heat treatment-driven microstructural evolution, mechanical properties, and electrochemical behavior of direct powder forged Al–10Si–0.3Mg alloy, Int. J. Miner. Metall. Mater., (2026). https://doi.org/10.1007/s12613-025-3221-8
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直接粉末锻造 Al–10Si–0.3Mg 合金的热处理驱动微观结构演变、力学性能及电化学行为表征

摘要: 本研究探讨了直接时效 (DA)、固溶处理 (ST) 以及 ST 后进行 DA (T6) 对直接粉末锻造 Al–10Si–0.3Mg 合金试样显微组织、力学性能和腐蚀性能的影响。使用光学显微镜、扫描电子显微镜和电子背散射衍射进行的显微组织分析表明:在 DA 试样中,由于扩散结合增强,200°C 直接时效 (DA-2) 表现出显著提升的硅 (Si) 颗粒分布均匀性和最小的颗粒间边界;ST 试样表现出部分 Si 溶解、较高的孔隙率并保留了颗粒间边界;T6 试样则表现出改善的微观结构均匀性和增强的 Si 析出。此外,力学性能评估表明,T6 处理(包括在 500°C 下进行 180 min的 ST,随后在 200°C 下进行 360 min的DA)产生了最高的拉伸强度 (207.15 MPa) 和延伸率 (5.02%),紧随其后的是在 200°C 下进行 360 min DA 的试样 (203.13 MPa 和 4.39%)。这些改进归因于 DA-2 处理带来的较低残余应力、较大扩散距离以及良好分散的 Si 颗粒。使用循环极化和阻抗谱进行的腐蚀分析表明了不同的电化学响应,其中 DA-2 导致最低的腐蚀电流和最高的阻抗,而 ST 导致最低的耐腐蚀性。总体而言,在 200°C 下进行 360 min的直接时效是最有效的热处理方式,它在力学性能和耐腐蚀性能之间提供了最佳的平衡。

 

Characterization of heat treatment-driven microstructural evolution, mechanical properties, and electrochemical behavior of direct powder forged Al–10Si–0.3Mg alloy

Abstract: This study investigated the effects of direct aging (DA), solution treatment (ST), and ST followed by DA (T6) on the microstructural, mechanical, and corrosion properties of direct powder forged Al–10Si–0.3Mg alloy specimens. Microstructural analyses conducted using optical microscopy, scanning electron microscopy, and electron backscatter diffraction revealed that among DA specimens, direct aging at 200°C (DA-2) exhibited significantly enhanced silicon (Si) particle distribution uniformity and minimal interparticle boundaries owing to increased diffusion bonding; ST specimens exhibited partial Si dissolution, higher porosity, and retained the interparticle boundaries; and T6 specimens exhibited improved microstructural uniformity and enhanced Si precipitation. Furthermore, mechanical property evaluations indicated that T6 treatment comprising ST at 500°C for 180 min followed by DA at 200°C for 360 min resulted in the highest tensile strength (207.15 MPa) and elongation (5.02%), followed closely by DA at 200°C for 360 min (203.13 MPa and 4.39%). These improvements were attributed to the lower residual stress, higher diffusion distances, and well-dispersed Si particles induced by DA-2 treatment. Corrosion analyses conducted using cyclic polarization and impedance spectroscopy indicated varied electrochemical responses, with DA-2 resulting in the lowest corrosion current and highest impedance, and ST resulting in the lowest corrosion resistance. Overall, DA at 200°C for 360 min was the most effective heat treatment, offering the optimal balance between mechanical and corrosion-resistance properties.

 

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