YE Yaping, ZHOU Keyan, GAO Thznxian, SUN Yu, and LU Bingling, Preparation of Nanometric Particles of Aluminum Nitride by Pyrolysis of Diethylaluminun Azide, J. Univ. Sci. Technol. Beijing, 4(1997), No. 4, pp. 43-46.
Cite this article as:
YE Yaping, ZHOU Keyan, GAO Thznxian, SUN Yu, and LU Bingling, Preparation of Nanometric Particles of Aluminum Nitride by Pyrolysis of Diethylaluminun Azide, J. Univ. Sci. Technol. Beijing, 4(1997), No. 4, pp. 43-46.
YE Yaping, ZHOU Keyan, GAO Thznxian, SUN Yu, and LU Bingling, Preparation of Nanometric Particles of Aluminum Nitride by Pyrolysis of Diethylaluminun Azide, J. Univ. Sci. Technol. Beijing, 4(1997), No. 4, pp. 43-46.
Citation:
YE Yaping, ZHOU Keyan, GAO Thznxian, SUN Yu, and LU Bingling, Preparation of Nanometric Particles of Aluminum Nitride by Pyrolysis of Diethylaluminun Azide, J. Univ. Sci. Technol. Beijing, 4(1997), No. 4, pp. 43-46.
Applied Science School, USTB, Beijing 100083, China
School of Chemical Engineering, Dalian University of Technology
中文摘要
Thermal stabilities of diethylaluminum azide were studied by means of theoretical analysis and expriments.The results have shown that diethylaluminum and azid be heated to vigorous refluxing under vacuum(400 Pa) at temperature as high as 420℃ without incident of explosion and decomposes smoothly during 460~580℃ to form nanometric particles of aluminum nitride in the aerosol synthesis reactor. A new way of preparing nanometric parties of aluminum nitrideis found.
Thermal stabilities of diethylaluminum azide were studied by means of theoretical analysis and expriments.The results have shown that diethylaluminum and azid be heated to vigorous refluxing under vacuum(400 Pa) at temperature as high as 420℃ without incident of explosion and decomposes smoothly during 460~580℃ to form nanometric particles of aluminum nitride in the aerosol synthesis reactor. A new way of preparing nanometric parties of aluminum nitrideis found.
下载: