Cite this article as: |
Qian Zhou, Juan-hong Liu, Ai-xiang Wu, and Hong-jiang Wang, Early-age strength property improvement and stability analysis of unclassified tailing paste backfill materials, Int. J. Miner. Metall. Mater., 27(2020), No. 9, pp. 1191-1202. https://doi.org/10.1007/s12613-020-1977-4 |
Juan-hong Liu E-mail: juanhong1966@hotmail.com
High-density tailings, small cementitious materials, and additives are used for backfill materials with poor early compressive strength (ECS), which may greatly affect the mining and backfill cycle, to prepare paste backfill materials (PBMs) with a high ECS. The effects and mechanisms of different early strength agents on the property of PBM are investigated. The action mechanism of additives on the properties of PBM is also analyzed through X-ray diffraction, scanning electron microscope, and energy dispersive spectrometry. Results show that the effects of single-component additives 1, 3, and 6 are better than those of the other additives, and their optimal dosages are 3wt%, 1wt%, and 3wt%, respectively. The optimum multicomponent combinations are 1wt% of additive 1 and 1.5wt% of additive 6. The ECS of the paste with additive 10 increases to a greater extent than that of the other pastes because of the synergistic action of additive 1 with additive 6. The hydration product of Ca(OH)2 is consumed, and more C–S–H gels are generated with the addition of additives to paste. Tailings particles, ettringite crystals, and gels intertwined with one another form a dense net-like structure that fills the pores. This structure can significantly improve the ECS of PBM.
[1] |
Z.F. Bian, X.X. Miao, S.G. Lei, S.E. Chen, W.F. Wang, and S. Struthers, The challenges of reusing mining and mineral-processing wastes, Science, 337(2012), No. 6095, p. 702. doi: 10.1126/science.1224757
|
[2] |
M. Fall, J.C. Célestin, M. Pokharel, and M. Touré, A contribution to understanding the effects of curing temperature on the mechanical properties of mine cemented tailings backfill, Eng. Geol., 114(2010), No. 3-4, p. 397. doi: 10.1016/j.enggeo.2010.05.016
|
[3] |
W. Sun, A.X. Wu, K.P. Hou, Y. Yang, L. Liu, and Y.M. Wen, Experimental study on the microstructure evolution of mixed disposal paste in surface subsidence areas, Minerals, 6(2016), No. 2, p. 43. doi: 10.3390/min6020043
|
[4] |
W.B. Xu, P.W. Cao, and M.M. Tian, Strength development and microstructure evolution of cemented tailings backfill containing different binder types and contents, Minerals, 8(2018), No. 4, p. 167. doi: 10.3390/min8040167
|
[5] |
A.X. Wu, Y. Yang, H.Y. Cheng, S.M. Chen, and Y. Han, Status and prospects of paste technology in China, Chin. J. Eng., 40(2018), No. 5, p. 517.
|
[6] |
J.H. Liu, Y.C. Zhou, A.X. Wu, and H.J. Wang, Reconstruction of broken Si–O–Si bonds in iron ore tailings (IOTs) in concrete, Int. J. Miner. Metall. Mater., 26(2019), No. 10, p. 1329. doi: 10.1007/s12613-019-1811-z
|
[7] |
S.H. Yin, Y.J. Shao, A.X. Wu, Y.M. Wang, and X. Chen, Expansion and strength properties of cemented backfill using sulphidic mill tailings, Constr. Build. Mater., 165(2018), p. 138. doi: 10.1016/j.conbuildmat.2018.01.005
|
[8] |
B. Koohestani, B. Bussiere, T. Belem, and A. Koubaa, Influence of polymer powder on properties of cemented paste backfill, Int. J. Miner. Process., 167(2017), p. 1. doi: 10.1016/j.minpro.2017.07.013
|
[9] |
J.Y. Wu, M.M. Feng, Z.Q. Chen, X.B. Mao, G.S. Han, and Y.M. Wang, Particle size distribution effects on the strength characteristic of cemented paste backfill, Minerals, 8(2018), No. 8, p. 322. doi: 10.3390/min8080322
|
[10] |
S. Cao, E. Yilmaz, and W.D. Song, Evaluation of viscosity, strength and microstructural properties of cemented tailings backfill, Minerals, 8(2018), No. 8, p. 352. doi: 10.3390/min8080352
|
[11] |
E. Yilmaz, T. Belem, and M. Benzaazoua, Study of physico-chemical and mechanical characteristics of consolidated and unconsolidated cemented paste backfills, Gospod. Surowcami Miner, 29(2013), No. 1, p. 81. doi: 10.2478/gospo-2013-0006
|
[12] |
E. Yilmaz, Stope depth effect on field behaviour and performance of cemented paste backfills, Int. J. Min. Reclam. Environ., 32(2018), No. 4, p. 273. doi: 10.1080/17480930.2017.1285858
|
[13] |
S. Cao, E. Yilmaz, and W.D. Song, Dynamic response of cement-tailings matrix composites under SHPB compression load, Constr. Build. Mater., 186(2018), p. 892. doi: 10.1016/j.conbuildmat.2018.08.009
|
[14] |
X. Zhao, A. Fourie, and C.C. Qi, An analytical solution for evaluating the safety of an exposed face in a paste backfill stope incorporating the arching phenomenon, Int. J. Miner. Metall. Mater., 26(2019), No. 10, p. 1206. doi: 10.1007/s12613-019-1885-7
|
[15] |
A.X. Wu, Y. Wang, H.J. Wang, S.H. Yin, and X.X. Miao, Coupled effects of cement type and water quality on the properties of cemented paste backfill, Int. J. Miner. Process., 143(2015), p. 65. doi: 10.1016/j.minpro.2015.09.004
|
[16] |
J.X. Fu, W.D. Song, Y.Y. Tan, and C.C. Sorrell, Study on microstructural evolution and strength growth and fracture mechanism of cemented paste backfill, Adv. Mater. Sci. Eng., 2016(2016), art. No. 8792817.
|
[17] |
J.R. Zheng, L.J. Guo, X.X. Sun, W.C. Li, and Q. Jia, Study on the strength development of cemented backfill body from lead-zinc mine tailings with sulphide, Adv. Mater. Sci. Eng., 2018(2018), art. No. 7278014.
|
[18] |
Y.Y. Tan, X. Yu, D. Elmo, L.H. Xu, and W.D. Song, Experimental study on dynamic mechanical property of cemented tailings backfill under SHPB impact loading, Int. Miner. Metall. Mater., 26(2019), No. 4, p. 404. doi: 10.1007/s12613-019-1749-1
|
[19] |
E. Yilmaz, T. Belem, B. Bussière, and M. Benzaazoua, Relationships between microstructural properties and compressive strength of consolidated and unconsolidated cemented paste backfills, Cem. Concr. Compos., 33(2011), No. 6, p. 702. doi: 10.1016/j.cemconcomp.2011.03.013
|
[20] |
F. Cihangir, B. Ercikdi, A. Kesimal, H. Deveci, and F. Erdemir, Paste backfill of high-sulphide mill tailings using alkali-activated blast furnace slag: Effect of activator nature, concentration and slag properties, Miner. Eng., 83(2015), p. 117. doi: 10.1016/j.mineng.2015.08.022
|
[21] |
A. Tariq and E.K. Yanful, A review of binders used in cemented paste tailings for underground and surface disposal practices, J. Environ. Manage., 131(2013), p. 138. doi: 10.1016/j.jenvman.2013.09.039
|
[22] |
H.Z. Jiao, S.F. Wang, A.X. Wu, H.M. Shen, and J.D. Wang, Cementitious property of NaAlO2-activated Ge slag as cement supplement, Int. J. Miner. Metall. Mater., 26(2019), No. 12, p. 1594. doi: 10.1007/s12613-019-1901-y
|
[23] |
L. Yang, J.P. Qiu, H.Q. Jiang, S.Q. Hu, H. Li, and S.B. Li, Use of cemented super-fine unclassified tailings backfill for control of subsidence, Minerals, 7(2017), No. 11, p. 216. doi: 10.3390/min7110216
|
[24] |
J.P. Qiu, L. Yang, X.G. Sun, J. Xing, and S.B. Li, Strength characteristics and failure mechanism of cemented super-fine unclassified tailings backfill, Minerals, 7(2017), No. 4, p. 58. doi: 10.3390/min7040058
|
[25] |
X. Chen, X. Shi, J. Zhou, X.H. Du, Q.S. Chen, and X.Y. Qiu, Effect of overflow tailings properties on cemented paste backfill, J. Environ. Manage., 235(2019), p. 133. doi: 10.1016/j.jenvman.2019.01.040
|
[26] |
W.C. Li and M. Fall, Sulphate effect on the early age strength and self-desiccation of cemented paste backfill, Constr. Build. Mater., 106(2016), p. 296. doi: 10.1016/j.conbuildmat.2015.12.124
|
[27] |
O. Nasir and M. Fall, Coupling binder hydration, temperature and compressive strength development of underground cemented paste backfill at early ages, Tunnelling Underground Space Technol., 25(2010), No. 1, p. 9. doi: 10.1016/j.tust.2009.07.008
|
[28] |
Y. Wang, M. Fall, and A.X. Wu, Initial temperature-dependence of strength development and self-desiccation in cemented paste backfill that contains sodium silicate, Cem. Concr. Compos., 67(2016), p. 101. doi: 10.1016/j.cemconcomp.2016.01.005
|
[29] |
S.H. Yin, A.X. Wu, K.J. Hu, Y. Wang, and Y.K. Zhang, The effect of solid components on the rheological and mechanical properties of cemented paste backfill, Miner. Eng., 35(2012), p. 61. doi: 10.1016/j.mineng.2012.04.008
|
[30] |
G.Z. Jiang, A.X Wu, Y. Wang, and W.T. Lan, Low cost and high efficiency utilization of hemihydrate phosphogypsum: Used as binder to prepare filling material, Constr. Build. Mater., 167(2018), p. 263. doi: 10.1016/j.conbuildmat.2018.02.022
|
[31] |
Y. Liu, C. Lu, H.Q. Zhang, and J.P. Li, Experimental study on chemical activation of recycled powder as a cementitious material in mine paste backfilling, Environ. Eng. Res., 21(2016), No. 4, p. 341. doi: 10.4491/eer.2015.129
|
[32] |
B. Koohestani, T. Belem, A. Koubaa, and B. Bussière, Experimental investigation into the compressive strength development of cemented paste backfill containing Nano-silica, Cem. Concr. Compos., 72(2016), p. 180. doi: 10.1016/j.cemconcomp.2016.06.016
|
[33] |
B. Koohestani, A. Koubaa, T. Belem, B. Bussière, and H. Bouzahzah, Experimental investigation of mechanical and microstructural properties of cemented paste backfill containing maple-wood filler, Constr. Build. Mater., 121(2016), p. 222. doi: 10.1016/j.conbuildmat.2016.05.118
|
[34] |
L. Yang, E. Yilmaz, J.W. Li, H. Liu, and H.Q. Jiang, Effect of superplasticizer type and dosage on fluidity and strength behavior of cemented tailings backfill with different solid contents, Constr. Build. Mater., 187(2018), p. 290. doi: 10.1016/j.conbuildmat.2018.07.155
|
[35] |
B. Koohestani, A.K. Darban, and P. Mokhtari, A comparison between the influence of superplasticizer and organosilanes on different properties of cemented paste backfill, Constr. Build. Mater., 173(2018), p. 180. doi: 10.1016/j.conbuildmat.2018.03.265
|
[36] |
D. Ouattara, T. Belem, M. Mbonimpa, and A. Yahia, Effect of superplasticizers on the consistency and unconfined compressive strength of cemented paste backfills, Constr. Build. Mater., 181(2018), p. 59. doi: 10.1016/j.conbuildmat.2018.05.288
|
[37] |
J. Zhang, H.W. Deng, A. Taheri, J.R. Deng, and B. Ke, Effects of superplasticizer on the hydration, consistency, and strength development of cemented paste backfill, Minerals, 8(2018), No. 9, p. 381. doi: 10.3390/min8090381
|
[38] |
M.B.C. Mangane, R. Argane, R. Trauchessec, A. Lecomte, and M. Benzaazoua, Influence of superplasticizers on mechanical properties and workability of cemented paste backfill, Miner. Eng., 116(2018), p. 3. doi: 10.1016/j.mineng.2017.11.006
|
[39] |
B. Ercikdi, H. Baki, and M. Izki, Effect of desliming of sulphide-rich mill tailings on the long-term strength of cemented paste backfill, J. Environ Manage., 115(2013), p. 5. doi: 10.1016/j.jenvman.2012.11.014
|
[40] |
G.L. Xue, E. Yilmaz, W.D. Song, and S. Cao, Compressive strength characteristics of cemented tailings backfill with alkali-activated slag, Appl. Sci., 8(2018), No. 9, p. 1537. doi: 10.3390/app8091537
|
[41] |
H.Q. Jiang, Z.J. Qi, E. Yilmaz, J. Han, J.P. Qiu, and C.L. Dong, Effectiveness of alkali-activated slag as alternative binder on workability and early age compressive strength of cemented paste backfills, Constr. Build. Mater., 218(2019), p. 689. doi: 10.1016/j.conbuildmat.2019.05.162
|
[42] |
H.Q. Jiang, J. Han, Y.H. Li, E. Yilmaz, Q. Sun, and J.P. Liu, Relationship between ultrasonic pulse velocity and uniaxial compressive strength for cemented paste backfill with alkali-activated slag, Nondestr. Test. Eval. (2019). DOI: 10.1080/10589759.2019.1679140
|
[43] |
M. Gao, J.H. Liu, A.X. Wu, and X.H. Zhao, Corrosion and deterioration mechanism of rich-water filling materials in typical chloride salt environment, J. Cent. South. Univ. Sci. Technol., 47(2016), No. 8, p. 2776.
|
[44] |
A.X. Wu, Y. Wang, and H.J. Wang, Status and prospects of the paste backfill technology, Met. Mine, 2016, No. 7, p. 1.
|
[45] |
N.R. Yang and W.H. Yue, The Handbook of Inorganic Non-metallic Materials Atlas, Wuhan University of Technology Press, Wuhan, 2000, p. 4.
|
[46] |
D.P. Mishra and S.K. Das, One-dimensional consolidation of sedimented stowed pond ash and pond ash-lime mixture deposits-a comparative study, Part. Sci. Technol., 33(2015), No. 2, p. 172. doi: 10.1080/02726351.2014.947662
|