Kwang Tae Son, Chang Hee Cho, Myoung Gyun Kim,  and Ji Woon Lee, Two-stage dynamic recrystallization and texture evolution in Al–7Mg alloy during hot torsion, Int. J. Miner. Metall. Mater., 31(2024), No. 8, pp. 1900-1911. https://doi.org/10.1007/s12613-024-2877-9
Cite this article as:
Kwang Tae Son, Chang Hee Cho, Myoung Gyun Kim,  and Ji Woon Lee, Two-stage dynamic recrystallization and texture evolution in Al–7Mg alloy during hot torsion, Int. J. Miner. Metall. Mater., 31(2024), No. 8, pp. 1900-1911. https://doi.org/10.1007/s12613-024-2877-9
Research Article

Two-stage dynamic recrystallization and texture evolution in Al–7Mg alloy during hot torsion

+ Author Affiliations
  • Corresponding author:

    Ji Woon Lee    E-mail: jwl@kongju.ac.kr

  • Received: 8 January 2024Revised: 18 February 2024Accepted: 7 March 2024Available online: 8 March 2024
  • Hot torsion tests were performed on the Al–7Mg alloy at the temperature ranging from 300 to 500°C and strain rates between 0.05 and 5 s−1 to explore the progressive dynamic recrystallization (DRX) and texture behaviors. The DRX behavior of the alloy manifested two distinct stages: Stage 1 at strain of ≤2 and Stage 2 at strains of ≥2. In Stage 1, there was a slight increase in the DRXed grain fraction (XDRX) with predominance of discontinuous DRX (DDRX), followed by a modest change in XDRX until the transition to Stage 2. Stage 2 was marked by an accelerated rate of DRX, culminating in a substantial final XDRX of ~0.9. Electron backscattered diffraction (EBSD) analysis on a sample in Stage 2 revealed that continuous DRX (CDRX) predominantly occurred within the ($ 1 \bar{2} 1$) [001] grains, whereas the (111) [110] grains underwent a geometric DRX (GDRX) evolution without a noticeable sub-grain structure. Furthermore, a modified Avrami’s DRX kinetics model was utilized to predict the microstructural refinement in the Al–7Mg alloy during the DRX evolution. Although this kinetics model did not accurately capture the DDRX behavior in Stage 1, it effectively simulated the DRX rate in Stage 2. The texture index was employed to assess the evolution of the texture isotropy during hot-torsion test, demonstrating significant improvement (>75%) in texture randomness before the commencement of Stage 2. This initial texture evolution is attributed to the rotation of parent grains and the substructure evolution, rather than to an increase in XDRX.
  • loading
  • [1]
    F.J. Humphreys and M. Hatherly, Recrystallization and Related Annealing Phenomena, Elsevier, Amsterdam, 2004.
    [2]
    H.J. McQueen, S. Spigarelli, M.E. Kassner, and E. Evangelista, Hot Deformation and Processing of Aluminum Alloys, CRC Press, Boca Raton, 2016.
    [3]
    J.J. Jonas, Dynamic recrystallization—Scientific curiosity or industrial tool?, Mater. Sci. Eng. A, 184(1994), No. 2, p. 155. doi: 10.1016/0921-5093(94)91028-6
    [4]
    N. Ravichandran and Y.V.R.K. Prasad, Dynamic recrystallization during hot deformation of aluminum: A study using processing maps, Metall. Trans. A, 22(1991), No. 10, p. 2339. doi: 10.1007/BF02665000
    [5]
    L. Xing, P.F. Gao, M. Zhan, Z.P. Ren, and X.G. Fan, A micromechanics-based damage constitutive model considering microstructure for aluminum alloys, Int. J. Plast., 157(2022), art. No. 103390. doi: 10.1016/j.ijplas.2022.103390
    [6]
    K. Huang and R.E. Logé, A review of dynamic recrystallization phenomena in metallic materials, Mater. Des., 111(2016), p. 548. doi: 10.1016/j.matdes.2016.09.012
    [7]
    Y.C. Lin, X.H. Zhu, W.Y. Dong, H. Yang, Y.W. Xiao, and N. Kotkunde, Effects of deformation parameters and stress triaxiality on the fracture behaviors and microstructural evolution of an Al–Zn–Mg–Cu alloy, J. Alloys Compd., 832(2020), art. No. 154988. doi: 10.1016/j.jallcom.2020.154988
    [8]
    L.E. Murr, Interfacial Phenomena in Metal and Alloys, Addison-Wesley Pub. Co., Boston, 1975.
    [9]
    R.W. Hertzberg, R.P. Vinci, and J.L. Hertzberg, Deformation and Fracture Mechanics of Engineering Materials, John Wiley & Sons, Hoboken, 2020.
    [10]
    E.I. Galindo-Nava, J. Sietsma, and P.E.J. Rivera-Díaz-del-Castillo, Dislocation annihilation in plastic deformation: II. Kocks–Mecking analysis, Acta Mater., 60(2012), No. 6-7, p. 2615. doi: 10.1016/j.actamat.2012.01.028
    [11]
    E.I. Galindo-Nava and P.E.J. Rivera-Díaz-del-Castillo, Thermostatistical modelling of hot deformation in FCC metals, Int. J. Plast., 47(2013), p. 202. doi: 10.1016/j.ijplas.2013.02.002
    [12]
    W. Blum, Q. Zhu, R. Merkel, and H.J. McQueen, Geometric dynamic recrystallization in hot torsion of Al–5Mg–0.6Mn (AA5083), Mater. Sci. Eng. A, 205(1996), No. 1-2, p. 23. doi: 10.1016/0921-5093(95)09990-5
    [13]
    G.A. Henshall, M.E. Kassner, and H.J. McQueen, Dynamic restoration mechanisms in Al-5.8 At. Pct Mg deformed to large strains in the solute drag regime, Metall. Trans. A, 23(1992), No. 3, p. 881. doi: 10.1007/BF02675565
    [14]
    H.W. Son, J.C. Lee, C.H. Cho, and S.K. Hyun, Effect of Mg content on the dislocation characteristics and discontinuous dynamic recrystallization during the hot deformation of Al–Mg alloy, J. Alloys Compd., 887(2021), art. No. 161397. doi: 10.1016/j.jallcom.2021.161397
    [15]
    M. Zecevic, R.A. Lebensohn, R.J. McCabe, and M. Knezevic, Modelling recrystallization textures driven by intragranular fluctuations implemented in the viscoplastic self-consistent formulation, Acta Mater., 164(2019), p. 530. doi: 10.1016/j.actamat.2018.11.002
    [16]
    O. Engler, Texture and anisotropy in the Al–Mg alloy AA 5005–Part I: Texture evolution during rolling and recrystallization, Mater. Sci. Eng. A, 618(2014), p. 654. doi: 10.1016/j.msea.2014.08.037
    [17]
    S. Tamimi, G. Sivaswamy, I. Violatos, S. Moturu, S. Rahimi, and P. Blackwell, Modelling and experimentation of the evolution of texture in an Al–Mg alloy during earing cupping test, Procedia Eng., 207(2017), p. 1. doi: 10.1016/j.proeng.2017.10.728
    [18]
    O. Engler and S. Kalz, Simulation of earing profiles from texture data by means of a visco-plastic self-consistent polycrystal plasticity approach, Mater. Sci. Eng. A, 373(2004), No. 1-2, p. 350. doi: 10.1016/j.msea.2004.02.003
    [19]
    J. Wang, X.J. Zhang, X. Lu, Y.S. Yang, and Z.H. Wang, Microstructure, texture and mechanical properties of hot-rolled Mg–4Al–2Sn–0.5Y–0.4Nd alloy, J. Magnesium Alloys, 4(2016), No. 3, p. 207. doi: 10.1016/j.jma.2016.07.004
    [20]
    K. Yoshida, Y. Tadano, and M. Kuroda, Improvement in formability of aluminum alloy sheet by enhancing geometrical hardening, Comput. Mater. Sci., 46(2009), No. 2, p. 459. doi: 10.1016/j.commatsci.2009.03.034
    [21]
    M. Rezayat, M.H. Parsa, H. Mirzadeh, and J.M. Cabrera, Texture development during hot deformation of Al/Mg alloy reinforced with ceramic particles, J. Alloys Compd., 798(2019), p. 267. doi: 10.1016/j.jallcom.2019.05.233
    [22]
    K. Yoshida, T. Ishizaka, M. Kuroda, and S. Ikawa, The effects of texture on formability of aluminum alloy sheets, Acta Mater., 55(2007), No. 13, p. 4499. doi: 10.1016/j.actamat.2007.04.014
    [23]
    X. Zeng, X.G. Fan, H.W. Li, et al., Grain refinement in hot working of 2219 aluminium alloy: On the effect of deformation mode and loading path, Mater. Sci. Eng. A, 794(2020), art. No. 139905. doi: 10.1016/j.msea.2020.139905
    [24]
    I. Kovacs and P. Feltham, Determination of the work-hardening characteristics of metals at large strains by means of torsion, Phys. Status Solidi B, 3(1963), No. 12, p. 2379. doi: 10.1002/pssb.19630031219
    [25]
    H.W. Son, C.H. Cho, J.C. Lee, et al., Deformation banding and static recrystallization in high-strain-rate-torsioned Al–Mg alloy, J. Alloys Compd., 814(2020), art. No. 152311. doi: 10.1016/j.jallcom.2019.152311
    [26]
    J.C. Li, X.D. Wu, L.F. Cao, B. Liao, Y.C. Wang, and Q. Liu, Hot deformation and dynamic recrystallization in Al–Mg–Si alloy, Mater. Charact., 173(2021), art. No. 110976. doi: 10.1016/j.matchar.2021.110976
    [27]
    K.T. Son, J.W. Lee, T.K. Jung, et al., Evaluation of dynamic recrystallization behaviors in hot-extruded AA5083 through hot torsion tests, Met. Mater. Int., 23(2017), No. 1, p. 68. doi: 10.1007/s12540-017-6384-7
    [28]
    D. Odoh, Y. Mahmoodkhani, and M. Wells, Effect of alloy composition on hot deformation behavior of some Al–Mg–Si alloys, Vacuum, 149(2018), p. 248. doi: 10.1016/j.vacuum.2017.12.037
    [29]
    G.J. Baxter, Q. Zhu, and C.M. Sellars, Effects of magnesium content on hot deformation and subsequent recrystallization behavior of aluminum–magnesium alloys, [in] Proceedings of International Conference on Aluminum Alloys (ICAA ), 6(1998), p. 1233.
    [30]
    H.T. Jeong, S.H. Han, and W.J. Kim, Effects of large amounts of Mg (5–13 wt%) on hot compressive deformation behavior and processing maps of Al–Mg alloys, J. Alloys Compd., 788(2019), p. 1282. doi: 10.1016/j.jallcom.2019.02.293
    [31]
    D.L. Sang, R.D. Fu, and Y.J. Li, The hot deformation activation energy of 7050 aluminum alloy under three different deformation modes, Metals, 6(2016), No. 3, art. No. 49. doi: 10.3390/met6030049
    [32]
    S.F. Medina and C.A. Hernandez, Modelling of the dynamic recrystallization of austenite in low alloy and microalloyed steels, Acta Mater., 44(1996), No. 1, p. 165. doi: 10.1016/1359-6454(95)00154-6
    [33]
    V. Randle and O. Engler, Introduction to Texture Analysis : Macrotexture , Microtexture and Orientation Mapping, CRC Press, Boca Raton, 2000.
    [34]
    S.I. Kim and Y.C. Yoo, Dynamic recrystallization behavior of AISI 304 stainless steel, Mater. Sci. Eng. A, 311(2001), No. 1-2, p. 108. doi: 10.1016/S0921-5093(01)00917-0
    [35]
    S. Serajzadeh and A. Karimi Taheri, An investigation on the effect of carbon and silicon on flow behavior of steel, Mater. Des., 23(2002), No. 3, p. 271. doi: 10.1016/S0261-3069(01)00080-2
    [36]
    E.I. Poliak and J.J. Jonas, A one-parameter approach to determining the critical conditions for the initiation of dynamic recrystallization, Acta Mater., 44(1996), No. 1, p. 127. doi: 10.1016/1359-6454(95)00146-7
    [37]
    J.J. Jonas, X. Quelennec. L. Jiang, and É Martin, The Avrami kinetics of dynamic recrystallization, Acta Mater., 57(2009), No. 9, p. 2748. doi: 10.1016/j.actamat.2009.02.033
    [38]
    S. Gourdet and F. Montheillet, An experimental study of the recrystallization mechanism during hot deformation of aluminium, Mater. Sci. Eng. A, 283(2000), No. 1-2, p. 274. doi: 10.1016/S0921-5093(00)00733-4
    [39]
    T. Sakai, H. Miura, A. Goloborodko, and O. Sitdikov, Continuous dynamic recrystallization during the transient severe deformation of aluminum alloy 7475, Acta Mater., 57(2009), No. 1, p. 153. doi: 10.1016/j.actamat.2008.09.001
    [40]
    T. Sakai, A. Belyakov, R. Kaibyshev, H. Miura, and J.J. Jonas, Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions, Prog. Mater. Sci., 60(2014), p. 130. doi: 10.1016/j.pmatsci.2013.09.002
    [41]
    H. Yamagata, Y. Ohuchida, N. Saito, and M. Otsuka, Nucleation of new grains during discontinuous dynamic recrystallization of 99.998 mass% aluminum at 453 K, Scripta Mater., 45(2001), No. 9, p. 1055. doi: 10.1016/S1359-6462(01)01139-3
    [42]
    R. Kapoor, G.B. Reddy, and A. Sarkar, Discontinuous dynamic recrystallization in α-Zr, Mater. Sci. Eng. A, 718(2018), p. 104. doi: 10.1016/j.msea.2018.01.117
    [43]
    M. Mofarrehi, M. Javidani, and X.-G. Chen, Effect of Mn content on the hot deformation behavior and microstructure evolution of Al–Mg–Mn 5xxx alloys, Mater. Sci. Eng. A, 845(2022), art. No. 143217. doi: 10.1016/j.msea.2022.143217
    [44]
    A.G. Beer and M.R. Barnett, Microstructural development during hot working of Mg–3Al–1Zn, Metall. Mater. Trans. A, 38(2007), No. 8, p. 1856. doi: 10.1007/s11661-007-9207-5
    [45]
    A. Heidarzadeh, T. Saeid, V. Klemm, A. Chabok, and Y.T. Pei, Effect of stacking fault energy on the restoration mechanisms and mechanical properties of friction stir welded copper alloys, Mater. Des., 162(2019), p. 185. doi: 10.1016/j.matdes.2018.11.050
    [46]
    Y. Zhang and C.J.L. Wilson, Lattice rotation in polycrystalline aggregates and single crystals with one slip system: A numerical and experimental approach, J. Struct. Geol., 19(1997), No. 6, p. 875. doi: 10.1016/S0191-8141(97)00016-3
    [47]
    G. Winther, Slip systems extracted from lattice rotations and dislocation structures, Acta Mater., 56(2008), No. 9, p. 1919. doi: 10.1016/j.actamat.2007.12.026
    [48]
    S.Y. Li, P. Van Houtte, and S.R. Kalidindi, A quantitative evaluation of the deformation texture predictions for aluminium alloys from crystal plasticity finite element method, Modell. Simul. Mater. Sci. Eng., 12(2004), No. 5, p. 845. doi: 10.1088/0965-0393/12/5/006
    [49]
    O. Engler, E. Sachot, J.C. Ehrström, A. Reeves, and R. Shahani, Recrystallisation and texture in hot deformed aluminium alloy 7010 thick plates, Mater. Sci. Technol., 12(1996), No. 9, p. 717. doi: 10.1179/mst.1996.12.9.717
    [50]
    T. Khelfa, R. Lachhab, H. Azzeddine, et al., Effect of ECAP and subsequent annealing on microstructure, texture, and microhardness of an AA6060 aluminum alloy, J. Mater. Eng. Perform., 31(2022), No. 4, p. 2606. doi: 10.1007/s11665-021-06404-w
    [51]
    S. Naghdy, L. Kestens, S. Hertelé, and P. Verleysen, Evolution of microstructure and texture in commercial pure aluminum subjected to high pressure torsion processing, Mater. Charact., 120(2016), p. 285. doi: 10.1016/j.matchar.2016.09.012
    [52]
    Z. Chen, G.A. Sun, Y. Wu, et al., Multi-scale study of microstructure evolution in hot extruded nano-sized TiB2 particle reinforced aluminum composites, Mater. Des., 116(2017), p. 577. doi: 10.1016/j.matdes.2016.12.070
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(9)  / Tables(4)

    Share Article

    Article Metrics

    Article Views(305) PDF Downloads(37) Cited by()
    Proportional views

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return