Mingxia Diao, Chunhuan Guo, Tao Dong, Shewei Xin, Zhonggang Sun, Siyuan Zhang, Haolun Song, Zubin Chen, Fengchun Jiang, and Sergey Konovalov, Grain refinement of Ti5321G alloy created by ultrasonic energy field during laser powder direct energy deposition, Int. J. Miner. Metall. Mater., (2026). https://doi.org/10.1007/s12613-025-3247-y
Cite this article as: Mingxia Diao, Chunhuan Guo, Tao Dong, Shewei Xin, Zhonggang Sun, Siyuan Zhang, Haolun Song, Zubin Chen, Fengchun Jiang, and Sergey Konovalov, Grain refinement of Ti5321G alloy created by ultrasonic energy field during laser powder direct energy deposition, Int. J. Miner. Metall. Mater., (2026). https://doi.org/10.1007/s12613-025-3247-y

Grain refinement of Ti5321G alloy created by ultrasonic energy field during laser powder direct energy deposition

  • The ultrasonic energy field (UEF)-induced grain refinement mechanisms in laser powder direct energy deposition-manufactured Ti5321G alloys were systematically investigated in this study. This study focused on the interplay between recrystallization in the high-temperature solid deposition layers and the ultrasonic cavitation-acoustic streaming effects during molten pool solidification. A novel experimental design was developed to decouple these mechanisms by creating four distinct UEF action zones (without UEF-N, with UEF-S, with UEF-L, and with UEF-S+L) within a single-pass multilayer sample. This approach enabled the dual effects of UEF (recrystallization in solidified layers and ultrasonic cavitation-acoustic streaming effects in liquid pools) to be directly compared. The UEF significantly refined the microstructures, reducing the average grain size by 64.2% (from (399.6 ± 28.6) to (143.1 ± 16.1) μm) in the with UEF-S+L zone, while promoting columnar-to-equiaxed transition, with the equiaxed grain probability increasing from 11.1% (without UEF) to 53.8%. The texture intensity was reduced by approximately 52.4% and the mechanical properties were enhanced, achieving a 6.2% increase in yield strength ((702.0 ± 10.6) MPa) and 31.7% improvement in elongation. Crucially, this study revealed the synergistic effect of the dual-action mechanisms of UEF, where recrystallization and cavitation-acoustic streaming collectively enabled non-linear grain refinement. This study provides a strategy for microstructural control in additive manufacturing, eliminating the need for complex post-processing and thereby advancing the industrial application of high-performance titanium components.
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